1,8-dibenzyl-4,11-bis-(3-bromobenzyl)-1,4,8,11-tetraazacyclotetradecane

Base Information

Chemical Name:1,8-dibenzyl-4,11-bis-(3-bromobenzyl)-1,4,8,11-tetraazacyclotetradecane
CAS No.:1415908-02-9
Molecular Formula:C₃₈H₄₆Br₂N₄
Molecular Weight:718.618
Hs Code.:

Synonyms:1,8-dibenzyl-4,11-bis-(3-bromobenzyl)-1,4,8,11-tetraazacyclotetradecane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,8-dibenzyl-4,11-bis-(3-bromobenzyl)-1,4,8,11-tetraazacyclotetradecane

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Technology Process of 1,8-dibenzyl-4,11-bis-(3-bromobenzyl)-1,4,8,11-tetraazacyclotetradecane

There total 1 articles about 1,8-dibenzyl-4,11-bis-(3-bromobenzyl)-1,4,8,11-tetraazacyclotetradecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 823-78-9
meta-bromobenzyl bromide

: 214078-93-0
1,8-Dibenzyl-1,4,8,11-tetraazacyclotetradecane

: 1415908-02-9
1,8-dibenzyl-4,11-bis-(3-bromobenzyl)-1,4,8,11-tetraazacyclotetradecane

Guidance literature:: With sodium hydroxide; In dichloromethane; water; for 49h;
DOI:10.3998/ark.5550190.0013.713

Reference yield: 28.0%

: 1415908-02-9
1,8-dibenzyl-4,11-bis-(3-bromobenzyl)-1,4,8,11-tetraazacyclotetradecane

: 51545-05-2
1,3-bis(aminoethyl)adamantane

: 1415908-06-3
30,36-dibenzyl-1,8,20,27,30,36-hexaazaheptacyclo[25.6.6.1^3,7.1^11,15.1^11,17.1^13,17.1^21,25]tetra-tetraconta-3⁽⁴⁴⁾,4,6,21⁽⁴⁰⁾,22,24-hexaene

: 30,63,69,80-tetrabenzyl-1,8,20,27,30,34,41,53,60,63,69,80-dodecaazatridecacyclo[58.6.6.6^27,34.1^3,7.1^11,15.1^11,17.1^13,17.1^21,25.1^36,40.1^44,48.1^44,50.1^46,50.1^54,58]-octaoctaconta-3⁽⁸⁸⁾,4,6,21⁽⁸⁴⁾,22,24,36,⁽⁷⁷⁾,37,39,54⁽⁷³⁾,55,57-dodecaene

: C₁₅₆H₂₁₀N₁₈

Guidance literature:: With 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; bis(dibenzylideneacetone)-palladium⁽⁰⁾; sodium t-butanolate; In 1,4-dioxane; Reflux;
DOI:10.3998/ark.5550190.0013.713

Reference yield: 24.0%

: 4246-51-9
4,7,10-trioxa-1,13-diaminotridecane

: 1415908-02-9
1,8-dibenzyl-4,11-bis-(3-bromobenzyl)-1,4,8,11-tetraazacyclotetradecane

: 32,38-dibenzyl-12,15,18-trioxa-1,8,22,29,32,38-hexaazatetracyclo[27.6.6.1^3,7.1^23,27]tritetraconta-3⁽⁴³⁾,4,6,23⁽⁴²⁾,24,26-hexaene

: 32,67,73,81-tetrabenzyl-12,15,18,47,50,53-hexaoxa-1,8,22,29,32,36,43,57,64,67,73,81-dodecaazaheptacyclo[62.6.6.6^29,36.1^3,7.1^23,27.1^38,42.1^58,62]hexaoctaconta-3⁽⁸⁶⁾,4,6,23⁽⁸⁵⁾,24,26,38⁽⁷⁸⁾,39,41,58⁽⁷⁷⁾,59,61-dodecaene

Guidance literature:: With 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; bis(dibenzylideneacetone)-palladium⁽⁰⁾; sodium t-butanolate; In 1,4-dioxane; Inert atmosphere; Reflux;
DOI:10.3987/COM-14-S(K)71