2-O-Acetyl-4-O-benzoyl-3-O-trichloroacetimidoyl-α-L-rhamnopyranosyl trichloroacetimidate

Base Information

Chemical Name:2-O-Acetyl-4-O-benzoyl-3-O-trichloroacetimidoyl-α-L-rhamnopyranosyl trichloroacetimidate
CAS No.:226982-79-2
Molecular Formula:C₁₉H₁₈Cl₆N₂O₇
Molecular Weight:599.079
Hs Code.:

Synonyms:2-O-Acetyl-4-O-benzoyl-3-O-trichloroacetimidoyl-α-L-rhamnopyranosyl trichloroacetimidate

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Chemical Property of 2-O-Acetyl-4-O-benzoyl-3-O-trichloroacetimidoyl-α-L-rhamnopyranosyl trichloroacetimidate

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Technology Process of 2-O-Acetyl-4-O-benzoyl-3-O-trichloroacetimidoyl-α-L-rhamnopyranosyl trichloroacetimidate

There total 3 articles about 2-O-Acetyl-4-O-benzoyl-3-O-trichloroacetimidoyl-α-L-rhamnopyranosyl trichloroacetimidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 545-06-2
trichloroacetonitrile

: 2-O-Acetyl-4-O-benzoyl-α/β-L-rhamnopyranose

: 226982-79-2
2-O-Acetyl-4-O-benzoyl-3-O-trichloroacetimidoyl-α-L-rhamnopyranosyl trichloroacetimidate

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; Ambient temperature;
DOI:10.1055/s-1999-2736

Reference yield:

: 183613-29-8
allyl 2-O-acetyl-4-O-benzoyl-α-L-rhamnopyranoside

: 226982-79-2
2-O-Acetyl-4-O-benzoyl-3-O-trichloroacetimidoyl-α-L-rhamnopyranosyl trichloroacetimidate

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / PdCl₂ / methanol / Ambient temperature

2: 89 percent / DBU / CH₂Cl₂ / Ambient temperature

With 1,8-diazabicyclo[5.4.0]undec-7-ene; palladium dichloride; In methanol; dichloromethane;
DOI:10.1055/s-1999-2736

Reference yield:

: 226982-74-7
Benzoic acid (2S,3S,4R,5R,6R)-5-acetoxy-6-allyloxy-2-methyl-4-(2,2,2-trichloro-acetimidoyloxy)-tetrahydro-pyran-3-yl ester

: 226982-79-2
2-O-Acetyl-4-O-benzoyl-3-O-trichloroacetimidoyl-α-L-rhamnopyranosyl trichloroacetimidate

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / TsOH*H₂O / methanol; CH₂Cl₂ / 0.08 h / Ambient temperature

2: 76 percent / PdCl₂ / methanol / Ambient temperature

3: 89 percent / DBU / CH₂Cl₂ / Ambient temperature

With toluene-4-sulfonic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; palladium dichloride; In methanol; dichloromethane;
DOI:10.1055/s-1999-2736