C₃₆H₄₆N₄O₆S

Base Information

• Chemical Name: C₃₆H₄₆N₄O₆S
• CAS No.: 1622244-99-8
• Molecular Formula: C₃₆H₄₆N₄O₆S
• Molecular Weight: 662.85
• Mol file: 1622244-99-8.mol

Synonyms:C₃₆H₄₆N₄O₆S

Chemical Property of C₃₆H₄₆N₄O₆S

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₆H₄₆N₄O₆S

There total 6 articles about C₃₆H₄₆N₄O₆S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C15H21IN2O3 (1613038-76-8) → C36H46N4O6S (1622244-99-8)

Guidance literature:

Multi-step reaction with 4 steps

1: triethylamine; trans-bis(triphenylphosphine)palladium dichloride; copper(l) iodide / 8 h / 20 °C

2: triethylamine / tetrahydrofuran / 0.5 h / 0 °C

3: lithium bromide / 4 h / 20 °C

4: sodium sulfide / methanol

With sodium sulfide; copper(l) iodide; trans-bis(triphenylphosphine)palladium dichloride; triethylamine; lithium bromide; In tetrahydrofuran; methanol; 1: |Sonogashira Cross-Coupling;

DOI:10.1021/jo500771g

Reference yield:

C18H23BrN2O3 (1613038-81-5) → C36H46N4O6S (1622244-99-8)

Guidance literature:

With sodium sulfide; In methanol;

DOI:10.1021/jo500771g

Reference yield:

L-N-Boc-Ala (15761-38-3) → C36H46N4O6S (1622244-99-8)

Guidance literature:

Multi-step reaction with 5 steps

1: N-(3-dimethylaminopropyl)-N-ethylcarbodiimide

2: triethylamine; trans-bis(triphenylphosphine)palladium dichloride; copper(l) iodide / 8 h / 20 °C

3: triethylamine / tetrahydrofuran / 0.5 h / 0 °C

4: lithium bromide / 4 h / 20 °C

5: sodium sulfide / methanol

With sodium sulfide; copper(l) iodide; trans-bis(triphenylphosphine)palladium dichloride; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; triethylamine; lithium bromide; In tetrahydrofuran; methanol; 2: |Sonogashira Cross-Coupling;

DOI:10.1021/jo500771g

upstream raw materials:

C₁₅H₂₁IN₂O₃

C₁₈H₂₃BrN₂O₃

2-iodobenzylamine

L-N-Boc-Ala

Downstream raw materials:

C₃₆H₄₆N₄O₈S