C₅₂H₅₀N₂O₇Si₂

Base Information

Chemical Name:C₅₂H₅₀N₂O₇Si₂
CAS No.:1352916-64-3
Molecular Formula:C₅₂H₅₀N₂O₇Si₂
Molecular Weight:871.149
Hs Code.:

C<sub>52</sub>H<sub>50</sub>N<sub>2</sub>O<sub>7</sub>Si<sub>2</sub>

Synonyms:C₅₂H₅₀N₂O₇Si₂

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Chemical Property of C₅₂H₅₀N₂O₇Si₂

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Technology Process of C₅₂H₅₀N₂O₇Si₂

There total 17 articles about C₅₂H₅₀N₂O₇Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 1352916-67-6
C₅₀H₄₈N₂O₆Si₂

: 108-24-7
acetic anhydride

: 1352916-64-3
C₅₂H₅₀N₂O₇Si₂

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 0 ℃; for 0.5h; Inert atmosphere;
DOI:10.1002/anie.201104504

Reference yield:

: C₅₃H₅₄N₂O₉SSi₂

: 1352916-64-3
C₅₂H₅₀N₂O₇Si₂

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1002/anie.201104504

Reference yield:

: 1352916-42-7
C₂₈H₃₈O₈Si

: 1352916-64-3
C₅₂H₅₀N₂O₇Si₂

Guidance literature:: Multi-step reaction with 11 steps

1.1: pyridine / 5.5 h / 20 °C / Inert atmosphere

2.1: lithium triethylborohydride / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

3.1: dmap / dichloromethane / 5 h / 20 °C / Inert atmosphere

4.1: pyridine; pyridine hydrogenfluoride / tetrahydrofuran / 15 h / 0 °C / Inert atmosphere

5.1: pyridine; Dess-Martin periodane / dichloromethane / 2 h / 20 °C / Inert atmosphere

6.1: sodium chlorite; disodium hydrogenphosphate; 2-methyl-but-2-ene / water; tert-butyl alcohol / 2 h / 0 °C / Inert atmosphere

7.1: trifluoroacetic anhydride / nitromethane / 2.5 h / 80 °C / Inert atmosphere; Molecular sieve

7.2: 2 h / 20 °C / Inert atmosphere

8.1: 1H-imidazole; dmap / dichloromethane / 20 h / 20 °C / Inert atmosphere

9.1: trifluoroacetic acid / water; isopropyl alcohol / 62 h / 20 °C / Inert atmosphere

10.1: ammonium cerium (IV) nitrate / acetonitrile / 1 h / 0 °C / pH 7 / Inert atmosphere; aq. buffer

11.1: triethylamine / dichloromethane / 1 h / 20 °C / Inert atmosphere

With pyridine; 1H-imidazole; dmap; sodium chlorite; disodium hydrogenphosphate; ammonium cerium (IV) nitrate; 2-methyl-but-2-ene; lithium triethylborohydride; Dess-Martin periodane; pyridine hydrogenfluoride; triethylamine; trifluoroacetic acid; trifluoroacetic anhydride; In tetrahydrofuran; nitromethane; dichloromethane; water; isopropyl alcohol; acetonitrile; tert-butyl alcohol; 7.1: Friedel Crafts acylation;
DOI:10.1002/anie.201104504