5-methyl-3-[2-methyl-4-(5-oxo-3-propyl-1-pyridin-2-yl-1,5-dihydro-[1,2,4]triazol-4-ylmethyl)-phenyl]-thiophene-2-sulfonic acid (4,5-dimethyl-isoxazol-3-yl)-(2-methoxy-ethoxymethyl)-amide

Base Information

Chemical Name:5-methyl-3-[2-methyl-4-(5-oxo-3-propyl-1-pyridin-2-yl-1,5-dihydro-[1,2,4]triazol-4-ylmethyl)-phenyl]-thiophene-2-sulfonic acid (4,5-dimethyl-isoxazol-3-yl)-(2-methoxy-ethoxymethyl)-amide
CAS No.:1214260-56-6
Molecular Formula:C₃₂H₃₈N₆O₆S₂
Molecular Weight:666.822
Hs Code.:

5-methyl-3-[2-methyl-4-(5-oxo-3-propyl-1-pyridin-2-yl-1,5-dihydro-[1,2,4]triazol-4-ylmethyl)-phenyl]-thiophene-2-sulfonic acid (4,5-dimethyl-isoxazol-3-yl)-(2-methoxy-ethoxymethyl)-amide

Synonyms:5-methyl-3-[2-methyl-4-(5-oxo-3-propyl-1-pyridin-2-yl-1,5-dihydro-[1,2,4]triazol-4-ylmethyl)-phenyl]-thiophene-2-sulfonic acid (4,5-dimethyl-isoxazol-3-yl)-(2-methoxy-ethoxymethyl)-amide

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Chemical Property of 5-methyl-3-[2-methyl-4-(5-oxo-3-propyl-1-pyridin-2-yl-1,5-dihydro-[1,2,4]triazol-4-ylmethyl)-phenyl]-thiophene-2-sulfonic acid (4,5-dimethyl-isoxazol-3-yl)-(2-methoxy-ethoxymethyl)-amide

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Technology Process of 5-methyl-3-[2-methyl-4-(5-oxo-3-propyl-1-pyridin-2-yl-1,5-dihydro-[1,2,4]triazol-4-ylmethyl)-phenyl]-thiophene-2-sulfonic acid (4,5-dimethyl-isoxazol-3-yl)-(2-methoxy-ethoxymethyl)-amide

There total 1 articles about 5-methyl-3-[2-methyl-4-(5-oxo-3-propyl-1-pyridin-2-yl-1,5-dihydro-[1,2,4]triazol-4-ylmethyl)-phenyl]-thiophene-2-sulfonic acid (4,5-dimethyl-isoxazol-3-yl)-(2-methoxy-ethoxymethyl)-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 948351-06-2
4-(4-bromo-3-methyl-benzyl)-5-propyl-2-pyridin-2-yl-2,4-dihydro-[1,2,4]triazol-3-one

: 948349-69-7
3-borono-N-(4,5-dimethyl-3-isoxazolyl)-N-[(2-methoxy-ethoxy)methyl]-5-methyl-thiophene sulphonamide

: 1214260-56-6
5-methyl-3-[2-methyl-4-(5-oxo-3-propyl-1-pyridin-2-yl-1,5-dihydro-[1,2,4]triazol-4-ylmethyl)-phenyl]-thiophene-2-sulfonic acid (4,5-dimethyl-isoxazol-3-yl)-(2-methoxy-ethoxymethyl)-amide

Guidance literature:: With sodium carbonate; bis-triphenylphosphine-palladium(II) chloride; In 1,2-dimethoxyethane; water; at 20 - 60 ℃; for 18.6667h; Heating / reflux;

Reference yield:

: 1214260-56-6
5-methyl-3-[2-methyl-4-(5-oxo-3-propyl-1-pyridin-2-yl-1,5-dihydro-[1,2,4]triazol-4-ylmethyl)-phenyl]-thiophene-2-sulfonic acid (4,5-dimethyl-isoxazol-3-yl)-(2-methoxy-ethoxymethyl)-amide

: 5-methyl-3-[2-methyl-4-(5-oxo-3-propyl-1-pyridin-2-yl-1,5-dihydro-[1,2,4]triazol-4-ylmethyl)-phenyl]-thiophene-2-sulfonic acid (4,5-dimethyl-isoxazol-3-yl)-amide

Guidance literature:: 5-methyl-3-[2-methyl-4-(5-oxo-3-propyl-1-pyridin-2-yl-1,5-dihydro-[1,2,4]triazol-4-ylmethyl)-phenyl]-thiophene-2-sulfonic acid (4,5-dimethyl-isoxazol-3-yl)-(2-methoxy-ethoxymethyl)-amide; With hydrogenchloride; water; In ethanol; at 20 ℃; for 3h; Heating / reflux;

With sodium hydrogencarbonate; In water; pH=8;