1,12-diiodoperfluorododecane

Base Information

• Chemical Name: 1,12-diiodoperfluorododecane
• CAS No.: 72049-11-7
• Molecular Formula: C₁₂F₂₄I₂
• Molecular Weight: 853.903

Synonyms:1,12-diiodoperfluorododecane

Chemical Property of 1,12-diiodoperfluorododecane

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

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Technology Process of 1,12-diiodoperfluorododecane

There total 9 articles about 1,12-diiodoperfluorododecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 22.7%

polytetrafluoroethylene (116-14-3,82785-14-6) → 1,2-diiodotetrafluoroethane (354-65-4) + 1,1,2,2,3,3,4,4-octafluoro-1,4-diiodobutane (375-50-8) + dodecafluoro-1,6-diiodohexane (375-80-4) + 1,12-diiodoperfluorododecane (72049-11-7)

Guidance literature:

With iodine; In neat (no solvent); at 200 - 220 ℃; for 22h; under 15200 - 20520 Torr; Further byproducts given;

DOI:10.1021/jo01290a030

Reference yield:

1,1,2,2,3,3-hexafluoro-1,3-diiodopropane (422-91-3) → dodecafluoro-1,6-diiodohexane (375-80-4) + 1H,9H-octadecafluoro-1,9-diiodo-nonane (22116-95-6) + 1,12-diiodoperfluorododecane (72049-11-7) + C9HF18I + 1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,12,12-Tetracosafluoro-1-iodo-dodecane

Guidance literature:

With cadmium; In acetonitrile; for 1h; Product distribution; Heating; other α,ω-diiodoperfluoroalkanes, var. solvent and temperature;

DOI:10.1016/S0022-1139(00)82187-9

Reference yield:

1,1,2,2,3,3,4,4-octafluoro-1,4-diiodobutane (375-50-8) → 1H,8H-perfluorooctane (307-99-3) + 1,12-diiodoperfluorododecane (72049-11-7) + 1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8-Hexadecafluoro-1-iodo-octane (79162-64-4) + 1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,12,12-Tetracosafluoro-1-iodo-dodecane

Guidance literature:

With cadmium; In acetonitrile; Further byproducts given;

DOI:10.1016/S0022-1139(00)81020-9

upstream raw materials:

polytetrafluoroethylene

1,1,2,2,3,3,4,4-octafluoro-1,4-diiodobutane

1,1,2,2,3,3-hexafluoro-1,3-diiodopropane

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