C₅₄H₅₆N₁₃O₁₂PS₆

Base Information

Chemical Name:C₅₄H₅₆N₁₃O₁₂PS₆
CAS No.:960062-84-4
Molecular Formula:C₅₄H₅₆N₁₃O₁₂PS₆
Molecular Weight:1302.49
Hs Code.:

C<sub>54</sub>H<sub>56</sub>N<sub>13</sub>O<sub>12</sub>PS<sub>6</sub>

Synonyms:C₅₄H₅₆N₁₃O₁₂PS₆

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₅₄H₅₆N₁₃O₁₂PS₆

Chemical Property:

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Technology Process of C₅₄H₅₆N₁₃O₁₂PS₆

There total 8 articles about C₅₄H₅₆N₁₃O₁₂PS₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 960062-83-3
C₅₈H₆₄N₁₃O₁₂PS₆

: 960062-84-4
C₅₄H₅₆N₁₃O₁₂PS₆

Guidance literature:: With trimethylsilyl bromide; In dichloromethane; at 0 - 20 ℃; for 2h;

Reference yield:

: GE₂₂₇₀ A

: 960062-84-4
C₅₄H₅₆N₁₃O₁₂PS₆

Guidance literature:: Multi-step reaction with 8 steps

1.1: water; sodium hydroxide / tetrahydrofuran / 1.5 h / 60 °C

2.1: chloroformic acid ethyl ester; triethylamine / acetone / 1 h

2.2: 1.33 h / 60 °C

3.1: 2 h / 80 °C

4.1: pyridine; dmap / 3 h

5.1: dichloromethane / 0.5 h

6.1: water; sodium hydrogencarbonate / ethyl acetate

7.1: pyridine

8.1: trimethylsilyl bromide / dichloromethane / 2 h / 0 - 20 °C

With pyridine; dmap; trimethylsilyl bromide; water; chloroformic acid ethyl ester; sodium hydrogencarbonate; triethylamine; sodium hydroxide; In tetrahydrofuran; dichloromethane; ethyl acetate; acetone;
DOI:10.1021/jm200938f

Reference yield:

: 960061-71-6
C₅₄H₅₅N₁₃O₁₀S₆

: 960062-84-4
C₅₄H₅₆N₁₃O₁₂PS₆

Guidance literature:: Multi-step reaction with 4 steps

1: dichloromethane / 0.5 h

2: water; sodium hydrogencarbonate / ethyl acetate

3: pyridine

4: trimethylsilyl bromide / dichloromethane / 2 h / 0 - 20 °C

With pyridine; trimethylsilyl bromide; water; sodium hydrogencarbonate; In dichloromethane; ethyl acetate;
DOI:10.1021/jm200938f