1α-methyl-1β-oxazolinyl-2β-(5-hydroxypentane)-3,4-dehydro-5-methoxytetralin

Base Information

Chemical Name:1α-methyl-1β-oxazolinyl-2β-(5-hydroxypentane)-3,4-dehydro-5-methoxytetralin
CAS No.:114839-03-1
Molecular Formula:C₂₈H₃₅NO₄
Molecular Weight:449.59
Hs Code.:

Synonyms:1α-methyl-1β-oxazolinyl-2β-(5-hydroxypentane)-3,4-dehydro-5-methoxytetralin

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1α-methyl-1β-oxazolinyl-2β-(5-hydroxypentane)-3,4-dehydro-5-methoxytetralin

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Technology Process of 1α-methyl-1β-oxazolinyl-2β-(5-hydroxypentane)-3,4-dehydro-5-methoxytetralin

There total 3 articles about 1α-methyl-1β-oxazolinyl-2β-(5-hydroxypentane)-3,4-dehydro-5-methoxytetralin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7766-48-5
1-iodo-4-pentene

: 114839-03-1
1α-methyl-1β-oxazolinyl-2β-(5-hydroxypentane)-3,4-dehydro-5-methoxytetralin

Guidance literature:: Multi-step reaction with 3 steps

1: tert-butyllithium / pentane / 0.5 h / -85 °C

2: 1.) THF, pentane, -85 deg C, 4 h, 2.) THF, pentane, -85 deg C

With tert.-butyl lithium; In pentane;
DOI:10.1016/S0040-4020(01)89161-4

Reference yield:

: 114838-81-2
1α-methyl-1β-oxazolinyl-2β-(4-pentenyl)-3,4-dehydro-5-methoxy-tetralin

: 114839-03-1
1α-methyl-1β-oxazolinyl-2β-(5-hydroxypentane)-3,4-dehydro-5-methoxytetralin

Guidance literature:: Yield given. Multistep reaction;
DOI:10.1016/S0040-4020(01)89161-4

Reference yield:

: 54313-25-6
4-penten-1-yllithium

: 114839-03-1
1α-methyl-1β-oxazolinyl-2β-(5-hydroxypentane)-3,4-dehydro-5-methoxytetralin

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) THF, pentane, -85 deg C, 4 h, 2.) THF, pentane, -85 deg C

DOI:10.1016/S0040-4020(01)89161-4