C₄₃H₅₆O₉Si

Base Information

Chemical Name:C₄₃H₅₆O₉Si
CAS No.:1315567-99-7
Molecular Formula:C₄₃H₅₆O₉Si
Molecular Weight:744.998
Hs Code.:

C<sub>43</sub>H<sub>56</sub>O<sub>9</sub>Si

Synonyms:C₄₃H₅₆O₉Si

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Chemical Property of C₄₃H₅₆O₉Si

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Technology Process of C₄₃H₅₆O₉Si

There total 20 articles about C₄₃H₅₆O₉Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 1315567-80-6
C₄₃H₅₈O₁₀Si

: 1315567-99-7
C₄₃H₅₆O₉Si

Guidance literature:: With toluene-4-sulfonic acid; In methanol; N,N-dimethyl-formamide; at 200 ℃; Microwave irradiation;
DOI:10.1038/nchem.1074

Reference yield:

: 1315567-64-6
C₄₄H₄₈O₁₂

: 1315567-99-7
C₄₃H₅₆O₉Si

Guidance literature:: Multi-step reaction with 8 steps

1.1: potassium carbonate / methanol; water / 50 °C

1.2: 0 °C

2.1: 2,6-dimethylpyridine; trifluoromethylsulfonic anhydride / dichloromethane / -78 °C

2.2: 65 °C

3.1: ammonium chloride; zinc / ethanol / 160 °C / Microwave irradiation

4.1: pyridinium p-toluenesulfonate / dichloromethane / 40 °C

5.1: N-Bromosuccinimide; sodium hydrogencarbonate; dibenzoyl peroxide / tetrachloromethane; benzene / 70 °C

5.2: 20 °C

6.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C

7.1: dmap; triethylamine / dichloromethane / 20 °C

8.1: toluene-4-sulfonic acid / methanol; N,N-dimethyl-formamide / 200 °C / Microwave irradiation

With 2,6-dimethylpyridine; dmap; N-Bromosuccinimide; lithium aluminium tetrahydride; trifluoromethylsulfonic anhydride; pyridinium p-toluenesulfonate; sodium hydrogencarbonate; potassium carbonate; ammonium chloride; toluene-4-sulfonic acid; triethylamine; zinc; dibenzoyl peroxide; In tetrahydrofuran; methanol; tetrachloromethane; ethanol; dichloromethane; water; N,N-dimethyl-formamide; benzene;
DOI:10.1038/nchem.1074

Reference yield:

: 1315567-74-8
C₃₃H₅₂O₉Si

: 1315567-99-7
C₄₃H₅₆O₉Si

Guidance literature:: Multi-step reaction with 11 steps

1.1: 1H-imidazole; tert-butyldimethylsilyl chloride / dichloromethane / 20 °C

1.2: 20 °C

2.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 20 °C

3.1: cerium(III) chloride / tetrahydrofuran / -78 °C

4.1: potassium carbonate / methanol; water / 50 °C

4.2: 0 °C

5.1: 2,6-dimethylpyridine; trifluoromethylsulfonic anhydride / dichloromethane / -78 °C

5.2: 65 °C

6.1: ammonium chloride; zinc / ethanol / 160 °C / Microwave irradiation

7.1: pyridinium p-toluenesulfonate / dichloromethane / 40 °C

8.1: N-Bromosuccinimide; sodium hydrogencarbonate; dibenzoyl peroxide / tetrachloromethane; benzene / 70 °C

8.2: 20 °C

9.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C

10.1: dmap; triethylamine / dichloromethane / 20 °C

11.1: toluene-4-sulfonic acid / methanol; N,N-dimethyl-formamide / 200 °C / Microwave irradiation

With 1H-imidazole; 2,6-dimethylpyridine; dmap; N-Bromosuccinimide; lithium aluminium tetrahydride; cerium(III) chloride; trifluoromethylsulfonic anhydride; pyridinium p-toluenesulfonate; sodium hydrogencarbonate; potassium carbonate; ammonium chloride; Dess-Martin periodane; toluene-4-sulfonic acid; tert-butyldimethylsilyl chloride; triethylamine; zinc; dibenzoyl peroxide; In tetrahydrofuran; methanol; tetrachloromethane; ethanol; dichloromethane; water; N,N-dimethyl-formamide; benzene;
DOI:10.1038/nchem.1074