1-⁽¹³⁾C-4'-amino-3',5'-dichloroacetophenone hydrochloride

Base Information

Chemical Name:1-⁽¹³⁾C-4'-amino-3',5'-dichloroacetophenone hydrochloride
CAS No.:1319718-86-9
Molecular Formula:C₈H₇Cl₂NO*ClH
Molecular Weight:241.506
Hs Code.:

1-<sup>(13)</sup>C-4'-amino-3',5'-dichloroacetophenone hydrochloride

Synonyms:1-⁽¹³⁾C-4'-amino-3',5'-dichloroacetophenone hydrochloride

Suppliers and Price of 1-⁽¹³⁾C-4'-amino-3',5'-dichloroacetophenone hydrochloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-⁽¹³⁾C-4'-amino-3',5'-dichloroacetophenone hydrochloride

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Technology Process of 1-⁽¹³⁾C-4'-amino-3',5'-dichloroacetophenone hydrochloride

There total 2 articles about 1-⁽¹³⁾C-4'-amino-3',5'-dichloroacetophenone hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1319718-85-8
1-⁽¹³⁾C-4'-acetamidoacetophenone

: 1319718-86-9
1-⁽¹³⁾C-4'-amino-3',5'-dichloroacetophenone hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide / methanol / 20 h / 50 °C

2: hydrogenchloride; N-chloro-succinimide / water / 10 h / 50 °C

With hydrogenchloride; N-chloro-succinimide; sodium hydroxide; In methanol; water;
DOI:10.1016/j.tet.2011.05.118

Reference yield:

: 103-84-4
Acetanilid

: 1319718-86-9
1-⁽¹³⁾C-4'-amino-3',5'-dichloroacetophenone hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: aluminum (III) chloride / 1,2-dichloro-ethane / 24 h / 60 °C / Inert atmosphere

2: sodium hydroxide / methanol / 20 h / 50 °C

3: hydrogenchloride; N-chloro-succinimide / water / 10 h / 50 °C

With hydrogenchloride; aluminum (III) chloride; N-chloro-succinimide; sodium hydroxide; In methanol; water; 1,2-dichloro-ethane; 1: Friedel Crafts acylation;
DOI:10.1016/j.tet.2011.05.118