(3aR,6R,6aS,9aS,10bR)-6-Methoxy-2,8-diphenyl-3a,6,6a,9a,10,10b-hexahydro-4H-isoindolo[5,6-e]isoindole-1,3,5,7,9-pentaone

Base Information

Chemical Name:(3aR,6R,6aS,9aS,10bR)-6-Methoxy-2,8-diphenyl-3a,6,6a,9a,10,10b-hexahydro-4H-isoindolo[5,6-e]isoindole-1,3,5,7,9-pentaone
CAS No.:90330-55-5
Molecular Formula:C₂₇H₂₂N₂O₆
Molecular Weight:470.481
Hs Code.:

Synonyms:(3aR,6R,6aS,9aS,10bR)-6-Methoxy-2,8-diphenyl-3a,6,6a,9a,10,10b-hexahydro-4H-isoindolo[5,6-e]isoindole-1,3,5,7,9-pentaone

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Chemical Property of (3aR,6R,6aS,9aS,10bR)-6-Methoxy-2,8-diphenyl-3a,6,6a,9a,10,10b-hexahydro-4H-isoindolo[5,6-e]isoindole-1,3,5,7,9-pentaone

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Technology Process of (3aR,6R,6aS,9aS,10bR)-6-Methoxy-2,8-diphenyl-3a,6,6a,9a,10,10b-hexahydro-4H-isoindolo[5,6-e]isoindole-1,3,5,7,9-pentaone

There total 3 articles about (3aR,6R,6aS,9aS,10bR)-6-Methoxy-2,8-diphenyl-3a,6,6a,9a,10,10b-hexahydro-4H-isoindolo[5,6-e]isoindole-1,3,5,7,9-pentaone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 90330-54-4
(3aR,6S,6aS,9aS,10aS,10bR)-6-Methoxy-2,8-diphenyl-5,10a-bis-trimethylsilanyloxy-3a,4,6,6a,9a,10,10a,10b-octahydro-isoindolo[5,6-e]isoindole-1,3,7,9-tetraone

: 90330-55-5
(3aR,6R,6aS,9aS,10bR)-6-Methoxy-2,8-diphenyl-3a,6,6a,9a,10,10b-hexahydro-4H-isoindolo[5,6-e]isoindole-1,3,5,7,9-pentaone

Guidance literature:: With trifluoroacetic acid; In benzene;
DOI:10.1246/cl.1984.273

Reference yield:

: 71043-35-1
3-methoxymethylenepentane-2,4-dione

: 90330-55-5
(3aR,6R,6aS,9aS,10bR)-6-Methoxy-2,8-diphenyl-3a,6,6a,9a,10,10b-hexahydro-4H-isoindolo[5,6-e]isoindole-1,3,5,7,9-pentaone

Guidance literature:: Multi-step reaction with 3 steps

1: 82 percent / ZnCl₂, (C₂H₅)3N / benzene / 24 h / 40 °C

2: 62 percent / benzene / 20 h / 50 °C

3: 89 percent / CF₃CO₂H / benzene

With triethylamine; trifluoroacetic acid; zinc(II) chloride; In benzene;
DOI:10.1246/bcsj.57.3221

Reference yield:

: 90330-49-7
3-(methoxymethylene)-2,4-bis(trimethylsilyloxy)-1,4-pentadiene

: 90330-55-5
(3aR,6R,6aS,9aS,10bR)-6-Methoxy-2,8-diphenyl-3a,6,6a,9a,10,10b-hexahydro-4H-isoindolo[5,6-e]isoindole-1,3,5,7,9-pentaone

Guidance literature:: Multi-step reaction with 2 steps

1: 62 percent / benzene / 20 h / 50 °C

2: 89 percent / CF₃CO₂H / benzene

With trifluoroacetic acid; In benzene;
DOI:10.1246/bcsj.57.3221