(1R,2R,3R,4aS,8aS)-3-azido-1-{[(3,5-dimethoxyphenyl)sulfanyl]methyl}-2,5,5,8a-tetramethyldecahydronaphthalen-2-ol

Base Information

Chemical Name:(1R,2R,3R,4aS,8aS)-3-azido-1-{[(3,5-dimethoxyphenyl)sulfanyl]methyl}-2,5,5,8a-tetramethyldecahydronaphthalen-2-ol
CAS No.:1619984-30-3
Molecular Formula:C₂₃H₃₅N₃O₃S
Molecular Weight:433.615
Hs Code.:

Synonyms:(1R,2R,3R,4aS,8aS)-3-azido-1-{[(3,5-dimethoxyphenyl)sulfanyl]methyl}-2,5,5,8a-tetramethyldecahydronaphthalen-2-ol

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Chemical Property of (1R,2R,3R,4aS,8aS)-3-azido-1-{[(3,5-dimethoxyphenyl)sulfanyl]methyl}-2,5,5,8a-tetramethyldecahydronaphthalen-2-ol

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Technology Process of (1R,2R,3R,4aS,8aS)-3-azido-1-{[(3,5-dimethoxyphenyl)sulfanyl]methyl}-2,5,5,8a-tetramethyldecahydronaphthalen-2-ol

There total 7 articles about (1R,2R,3R,4aS,8aS)-3-azido-1-{[(3,5-dimethoxyphenyl)sulfanyl]methyl}-2,5,5,8a-tetramethyldecahydronaphthalen-2-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 1619984-29-0
(1aR,2R,2aS,6aS,7aS)-2-{[(3,5-dimethoxyphenyl)sulfanyl]methyl}-1a,2a,6,6-tetramethyldecahydronaphtho[2,3-b]oxirene

: 1619984-30-3
(1R,2R,3R,4aS,8aS)-3-azido-1-{[(3,5-dimethoxyphenyl)sulfanyl]methyl}-2,5,5,8a-tetramethyldecahydronaphthalen-2-ol

Guidance literature:: With sodium azide; ammonium chloride; In N,N-dimethyl-formamide; at 80 ℃; for 120h; Inert atmosphere;

Reference yield:

: 500-99-2
3,5-dimethoxyphenol

: 1619984-30-3
(1R,2R,3R,4aS,8aS)-3-azido-1-{[(3,5-dimethoxyphenyl)sulfanyl]methyl}-2,5,5,8a-tetramethyldecahydronaphthalen-2-ol

Guidance literature:: Multi-step reaction with 5 steps

1: 1,4-diaza-bicyclo[2.2.2]octane / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

2: neat (no solvent) / 3 h / 260 °C / Inert atmosphere

3: potassium hydroxide / methanol / 2 h / Reflux

4: caesium carbonate / N,N-dimethyl-formamide / 17 h / 80 °C / Inert atmosphere

5: sodium azide; ammonium chloride / N,N-dimethyl-formamide / 120 h / 80 °C / Inert atmosphere

With 1,4-diaza-bicyclo[2.2.2]octane; sodium azide; ammonium chloride; caesium carbonate; potassium hydroxide; In methanol; N,N-dimethyl-formamide;

Reference yield:

: 54839-88-2
S-(3,5-dimethoxyphenyl) dimethylthiocarbamate

: 1619984-30-3
(1R,2R,3R,4aS,8aS)-3-azido-1-{[(3,5-dimethoxyphenyl)sulfanyl]methyl}-2,5,5,8a-tetramethyldecahydronaphthalen-2-ol

Guidance literature:: Multi-step reaction with 3 steps

1: potassium hydroxide / methanol / 2 h / Reflux

2: caesium carbonate / N,N-dimethyl-formamide / 17 h / 80 °C / Inert atmosphere

3: sodium azide; ammonium chloride / N,N-dimethyl-formamide / 120 h / 80 °C / Inert atmosphere

With sodium azide; ammonium chloride; caesium carbonate; potassium hydroxide; In methanol; N,N-dimethyl-formamide;