Benzyl-2-acetamido-4,6-O-benzyliden-2-desoxy-3-O-phenoxythiocarbonyl-α-D-galactopyranosid

Base Information

• Chemical Name: Benzyl-2-acetamido-4,6-O-benzyliden-2-desoxy-3-O-phenoxythiocarbonyl-α-D-galactopyranosid
• CAS No.: 141019-76-3
• Molecular Formula: C₂₉H₂₉NO₇S
• Molecular Weight: 535.618

Synonyms:Benzyl-2-acetamido-4,6-O-benzyliden-2-desoxy-3-O-phenoxythiocarbonyl-α-D-galactopyranosid

Chemical Property of Benzyl-2-acetamido-4,6-O-benzyliden-2-desoxy-3-O-phenoxythiocarbonyl-α-D-galactopyranosid

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Technology Process of Benzyl-2-acetamido-4,6-O-benzyliden-2-desoxy-3-O-phenoxythiocarbonyl-α-D-galactopyranosid

There total 1 articles about Benzyl-2-acetamido-4,6-O-benzyliden-2-desoxy-3-O-phenoxythiocarbonyl-α-D-galactopyranosid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

benzyl 2-acetamido-4,6-O-benzylidene-2-deoxy-α-D-glucopyranoside (78246-81-8) + phenylcarbonochloridothioate (1005-56-7) → benzyl 2-acetamido-4,6-O-benzylidene-2-deoxy-3-O-phenoxythiocarbonyl-α-D-glucopyranoside (141019-76-3)

Guidance literature:

With dmap; In acetonitrile; for 15h; Ambient temperature;

DOI:10.1016/0008-6215(90)84053-W

Reference yield: 79.0%

benzyl 2-acetamido-4,6-O-benzylidene-2-deoxy-3-O-phenoxythiocarbonyl-α-D-glucopyranoside (141019-76-3) → benzyl 2-acetamido-4,6-O-benzylidene-2,3-dideoxy-α-D-ribo-hexopyranoside (79297-67-9)

Guidance literature:

With azobisisobutyronitrile; tri-n-butyl-tin hydride; In toluene; at 80 ℃; for 2h;

DOI:10.1016/0008-6215(90)84053-W

Reference yield: 79.0%

Benzyl-2-acetamido-4,6-O-benzyliden-2-desoxy-3-O-phenoxythiocarbonyl-α-D-galactopyranosid (141019-76-3) → Benzyl-2-acetamido-4,6-O-benzyliden-2,3-didesoxy-α-D-xylo-hexopyranosid (141115-66-4)

Guidance literature:

With azobisisobutyronitrile; tri-n-butyl-tin hydride; In toluene; at 80 ℃; for 2h;

upstream raw materials:

benzyl 2-acetamido-4,6-O-benzylidene-2-deoxy-α-D-glucopyranoside

phenylcarbonochloridothioate

Downstream raw materials:

benzyl 2-acetamido-4,6-O-benzylidene-2,3-dideoxy-α-D-ribo-hexopyranoside

benzyl 2-acetamido-2,3-dideoxy-α-D-ribo-hexopyranoside

benzyl 2-acetamido-4,6-di-O-acetyl-2,3-dideoxy-α-D-ribo-hexopyranoside

2-acetamido-4,6-di-O-acetyl-2,3-dideoxy-α-D-ribo-hexopyranosyl dibenzyl phosphate

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