(E)-1-methyl-2-butenyl phenyl sulfone

Base Information

Chemical Name:(E)-1-methyl-2-butenyl phenyl sulfone
CAS No.:97663-40-6
Molecular Formula:C₁₁H₁₄O₂S
Molecular Weight:210.297
Hs Code.:

Synonyms:(E)-1-methyl-2-butenyl phenyl sulfone

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Chemical Property of (E)-1-methyl-2-butenyl phenyl sulfone

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Technology Process of (E)-1-methyl-2-butenyl phenyl sulfone

There total 5 articles about (E)-1-methyl-2-butenyl phenyl sulfone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 27748-50-1
(E)-2-nitro-pent-2-ene

: 873-55-2
sodium benzenesulfonate

: 97663-40-6
(E)-1-methyl-2-butenyl phenyl sulfone

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine; 1,2-bis-(diphenylphosphino)ethane; In N,N-dimethyl-formamide; at 70 ℃; for 2h;
DOI:10.1021/jo00373a008

Reference yield: 81.0%

: 27748-51-2
(Z)-2-nitropent-2-ene

: 25932-11-0
benzenesulfinic acid sodium dihydrate

: 97663-40-6
(E)-1-methyl-2-butenyl phenyl sulfone

Guidance literature:: With triethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 1,2-bis-(diphenylphosphino)ethane; In N,N-dimethyl-formamide; at 70 ℃; for 2h; Product distribution; Study of the palladium catalyzed synthesis of allylic sulfones from various α-nitro olefins and sodium benzenesulfinate in presence of tertiary amine;
DOI:10.1246/cl.1985.229

Reference yield:

: 2004-70-8,17410-45-6,25212-15-1,64940-84-7
1-methylbuta-1,3-diene

: 873-55-2
sodium benzenesulfonate

: 82234-80-8
<(2-pentenyl)sulfonyl> benzene

: 96236-31-6
(Z)-Pent-2-enyl phenyl sulphone

: 97663-40-6
(E)-1-methyl-2-butenyl phenyl sulfone

: 100312-74-1
(Z)-1-methyl-2-butenyl phenyl sulfone

Guidance literature:: With carbon dioxide; palladium; In N,N-dimethyl-formamide; at 110 ℃; for 4h; under 11032.6 Torr; Yield given. Yields of byproduct given;
DOI:10.1246/bcsj.59.3705