C₃₃H₃₃N₅O₃S

Base Information

Chemical Name:C₃₃H₃₃N₅O₃S
CAS No.:1313236-63-3
Molecular Formula:C₃₃H₃₃N₅O₃S
Molecular Weight:579.723
Hs Code.:

C<sub>33</sub>H<sub>33</sub>N<sub>5</sub>O<sub>3</sub>S

Synonyms:C₃₃H₃₃N₅O₃S

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Chemical Property of C₃₃H₃₃N₅O₃S

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Technology Process of C₃₃H₃₃N₅O₃S

There total 7 articles about C₃₃H₃₃N₅O₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: (1-tosylindole-3-yl)methyl chloride

: 1313236-61-1
9-(quinoxalin-2-yl)-2,9-diazaspiro[5.5]undecan-1-one

: 1313236-63-3
C₃₃H₃₃N₅O₃S

Guidance literature:: 9-(quinoxalin-2-yl)-2,9-diazaspiro[5.5]undecan-1-one; With sodium hydride; In tetrahydrofuran; for 0.166667h; Reflux;

(1-tosylindole-3-yl)methyl chloride; In tetrahydrofuran; at 20 - 60 ℃; for 16h;

With ammonium chloride; In tetrahydrofuran; water; at 20 ℃;

Reference yield:

: 1448-87-9
2-chloroquinoxaline

: 1313236-63-3
C₃₃H₃₃N₅O₃S

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 18 h / 60 °C

2.1: sodium hydride / tetrahydrofuran / 0.17 h / Reflux

2.2: 16 h / 20 - 60 °C

2.3: 20 °C

With sodium hydride; potassium carbonate; In tetrahydrofuran; N,N-dimethyl-formamide;

Reference yield:

: 487-89-8,1228547-52-1
Indole-3-carboxaldehyde

: 1313236-63-3
C₃₃H₃₃N₅O₃S

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium hydroxide / 1,2-dimethoxyethane / 18 h / 20 °C

2.1: sodium tetrahydroborate; methanol / 18 h / 0 - 20 °C

3.1: trichlorophosphate / tetrahydrofuran / 3 h / 0 - 20 °C / Reflux

4.1: sodium hydride / tetrahydrofuran / 0.17 h / Reflux

4.2: 16 h / 20 - 60 °C

4.3: 20 °C

With methanol; sodium tetrahydroborate; sodium hydride; potassium hydroxide; trichlorophosphate; In tetrahydrofuran; 1,2-dimethoxyethane;