Technology Process of C38H61FN5O7PS2
There total 7 articles about C38H61FN5O7PS2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: triethylsilane; trifluoroacetic acid / dichloromethane / 1.5 h / 20 °C
2.1: triethylamine / dichloromethane / 0.17 h / 20 °C
3.1: tetrakis(triphenylphosphine) palladium(0); pyrrolidine / dichloromethane / 5.5 h / 20 °C
4.1: triethylamine; 4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride / methanol / 0.33 h / 20 °C
4.2: 1 h / 20 °C
5.1: methanol; N,N-dimethyl-formamide / 2 h / 20 °C
With
pyrrolidine; triethylsilane; tetrakis(triphenylphosphine) palladium(0); triethylamine; trifluoroacetic acid; 4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride;
In
methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2014.04.104
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: tetrakis(triphenylphosphine) palladium(0); pyrrolidine / dichloromethane / 5.5 h / 20 °C
2.1: triethylamine; 4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride / methanol / 0.33 h / 20 °C
2.2: 1 h / 20 °C
3.1: methanol; N,N-dimethyl-formamide / 2 h / 20 °C
With
pyrrolidine; tetrakis(triphenylphosphine) palladium(0); triethylamine; 4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride;
In
methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2014.04.104