(S)-2-{4-[(S)-1-(2-Methoxy-benzoylamino)-1,2-dimethyl-propyl]-[1,2,3]triazol-1-yl}-hexanoic acid

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Chemical Name:(S)-2-{4-[(S)-1-(2-Methoxy-benzoylamino)-1,2-dimethyl-propyl]-[1,2,3]triazol-1-yl}-hexanoic acid
CAS No.:869205-69-6
Molecular Formula:C₂₁H₃₀N₄O₄
Molecular Weight:402.494
Hs Code.:

Synonyms:(S)-2-{4-[(S)-1-(2-Methoxy-benzoylamino)-1,2-dimethyl-propyl]-[1,2,3]triazol-1-yl}-hexanoic acid

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Chemical Property of (S)-2-{4-[(S)-1-(2-Methoxy-benzoylamino)-1,2-dimethyl-propyl]-[1,2,3]triazol-1-yl}-hexanoic acid

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Technology Process of (S)-2-{4-[(S)-1-(2-Methoxy-benzoylamino)-1,2-dimethyl-propyl]-[1,2,3]triazol-1-yl}-hexanoic acid

There total 3 articles about (S)-2-{4-[(S)-1-(2-Methoxy-benzoylamino)-1,2-dimethyl-propyl]-[1,2,3]triazol-1-yl}-hexanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 64508-50-5
2-methoxybenzoic anhydride

: 869205-69-6
(S)-2-{4-[(S)-1-(2-Methoxy-benzoylamino)-1,2-dimethyl-propyl]-[1,2,3]triazol-1-yl}-hexanoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: aq. NaOH / CHCl₃ / 22 h / Heating

2: i-Pr₂NEt; CuI / tetrahydrofuran / 24 h

With sodium hydroxide; copper(l) iodide; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; chloroform;
DOI:10.1021/ja0547230

Reference yield:

: 579-75-9
2-Methoxybenzoic acid

: 869205-69-6
(S)-2-{4-[(S)-1-(2-Methoxy-benzoylamino)-1,2-dimethyl-propyl]-[1,2,3]triazol-1-yl}-hexanoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 61 percent / triphosgene; 2,4,6-collidine / tetrahydrofuran / 0 - 20 °C

2: aq. NaOH / CHCl₃ / 22 h / Heating

3: i-Pr₂NEt; CuI / tetrahydrofuran / 24 h

With 2,4,6-trimethyl-pyridine; sodium hydroxide; copper(l) iodide; bis(trichloromethyl) carbonate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; chloroform;
DOI:10.1021/ja0547230