5-[bis[2-[(methylsulfonyl)oxy]ethyl]amino]-N-hydroxy-2,4-nitrobenzamide

Base Information

Chemical Name:5-[bis[2-[(methylsulfonyl)oxy]ethyl]amino]-N-hydroxy-2,4-nitrobenzamide
CAS No.:935431-05-3
Molecular Formula:C₁₃H₁₈N₄O₁₂S₂
Molecular Weight:486.438
Hs Code.:

Synonyms:5-[bis[2-[(methylsulfonyl)oxy]ethyl]amino]-N-hydroxy-2,4-nitrobenzamide

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Chemical Property of 5-[bis[2-[(methylsulfonyl)oxy]ethyl]amino]-N-hydroxy-2,4-nitrobenzamide

Chemical Property:

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Technology Process of 5-[bis[2-[(methylsulfonyl)oxy]ethyl]amino]-N-hydroxy-2,4-nitrobenzamide

There total 4 articles about 5-[bis[2-[(methylsulfonyl)oxy]ethyl]amino]-N-hydroxy-2,4-nitrobenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: methanesulfonic acid 2-[(5-chlorocarbonyl-2,4-dinitro-phenyl)-(2-methanesulfonyloxy-ethyl)-amino]-ethyl ester

: 935431-05-3
5-[bis[2-[(methylsulfonyl)oxy]ethyl]amino]-N-hydroxy-2,4-nitrobenzamide

Guidance literature:: With hydroxylamine hydrochloride; sodium carbonate; In diethyl ether; water; at 20 ℃; for 0.25h;
DOI:10.1021/jm061062o

Reference yield:

: 680199-24-0
5-(bis{2-[(methylsulfonyl)oxy]ethyl}amino)-2,4-dinitrobenzoic acid

: 935431-05-3
5-[bis[2-[(methylsulfonyl)oxy]ethyl]amino]-N-hydroxy-2,4-nitrobenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: SOCl₂; DMF / 1 h / Heating

2: hydroxylamine hydrochloride; Na₂CO₃ / diethyl ether; H₂O / 0.25 h / 20 °C

With thionyl chloride; hydroxylamine hydrochloride; sodium carbonate; N,N-dimethyl-formamide; In diethyl ether; water;
DOI:10.1021/jm061062o

Reference yield:

: 150272-09-6
methyl 5--2,4-dinitrobenzoate

: 935431-05-3
5-[bis[2-[(methylsulfonyl)oxy]ethyl]amino]-N-hydroxy-2,4-nitrobenzamide

Guidance literature:: Multi-step reaction with 4 steps

1: 92 percent / Et₃N; aq. KHCO₃ / CH₂Cl₂ / 0.5 h / 0 °C

2: KOH / dioxane; methanol / 0.25 h / 20 °C

3: SOCl₂; DMF / 1 h / Heating

4: hydroxylamine hydrochloride; Na₂CO₃ / diethyl ether; H₂O / 0.25 h / 20 °C

With potassium hydroxide; thionyl chloride; hydroxylamine hydrochloride; sodium carbonate; potassium hydrogencarbonate; triethylamine; N,N-dimethyl-formamide; In 1,4-dioxane; methanol; diethyl ether; dichloromethane; water;
DOI:10.1021/jm061062o