N-<3-<4-<2-(Benzyloxycarbonylamino)ethyl>phenoxy>-N-tert-butoxycarbonyl-(2R,3R)-prolyl>-(S)-prolin-pentafluorophenyl-ester

Base Information

Chemical Name:N-<3-<4-<2-(Benzyloxycarbonylamino)ethyl>phenoxy>-N-tert-butoxycarbonyl-(2R,3R)-prolyl>-(S)-prolin-pentafluorophenyl-ester
CAS No.:76847-34-2
Molecular Formula:C₃₇H₃₈F₅N₃O₈
Molecular Weight:747.716
Hs Code.:

Synonyms:N-<3-<4-<2-(Benzyloxycarbonylamino)ethyl>phenoxy>-N-tert-butoxycarbonyl-(2R,3R)-prolyl>-(S)-prolin-pentafluorophenyl-ester

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Chemical Property of N-<3-<4-<2-(Benzyloxycarbonylamino)ethyl>phenoxy>-N-tert-butoxycarbonyl-(2R,3R)-prolyl>-(S)-prolin-pentafluorophenyl-ester

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Technology Process of N-<3-<4-<2-(Benzyloxycarbonylamino)ethyl>phenoxy>-N-tert-butoxycarbonyl-(2R,3R)-prolyl>-(S)-prolin-pentafluorophenyl-ester

There total 14 articles about N-<3-<4-<2-(Benzyloxycarbonylamino)ethyl>phenoxy>-N-tert-butoxycarbonyl-(2R,3R)-prolyl>-(S)-prolin-pentafluorophenyl-ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 771-61-9
2,3,4,5,6-pentafluorophenol

: 76847-33-1
N-<3-<4-<2-(Benzyloxycarbonylamino)ethyl>phenoxy>-N-tert-butoxycarbonyl-(2R,3R)-prolyl>-(S)-prolin

: 76847-34-2
N-<3-<4-<2-(Benzyloxycarbonylamino)ethyl>phenoxy>-N-tert-butoxycarbonyl-(2R,3R)-prolyl>-(S)-prolin-pentafluorophenyl-ester

Guidance literature:: With dicyclohexyl-carbodiimide; In ethyl acetate; for 8h; Ambient temperature;
DOI:10.1002/jlac.198219821206

Reference yield:

: 84426-16-4
N-tert-Butoxycarbonyl-trans-3-<4-(cyanmethyl)phenoxy>prolin

: 76847-34-2
N-<3-<4-<2-(Benzyloxycarbonylamino)ethyl>phenoxy>-N-tert-butoxycarbonyl-(2R,3R)-prolyl>-(S)-prolin-pentafluorophenyl-ester

Guidance literature:: Multi-step reaction with 5 steps

2: H₂ / Pd/C / dioxane

3: 10 percent NH₂ / Rh/Al₂O₃ / ethanol / 2250.2 Torr

5: 83 percent / DCCD

With hydrogen; dicyclohexyl-carbodiimide; palladium on activated charcoal; Rh/Al₂O₃; In 1,4-dioxane; ethanol;

Reference yield:

: 84426-18-6
N--(S)-prolin

: 76847-34-2
N-<3-<4-<2-(Benzyloxycarbonylamino)ethyl>phenoxy>-N-tert-butoxycarbonyl-(2R,3R)-prolyl>-(S)-prolin-pentafluorophenyl-ester

Guidance literature:: Multi-step reaction with 3 steps

1: 10 percent NH₂ / Rh/Al₂O₃ / ethanol / 2250.2 Torr

3: 83 percent / DCCD

With dicyclohexyl-carbodiimide; Rh/Al₂O₃; In ethanol;