4,6-Dimethoxy-6'-methyl-5-nitro-4'-(3-nitro-phenyl)-2'-phenyl-1',4'-dihydro-[2,5']bipyrimidinyl

Base Information

Chemical Name:4,6-Dimethoxy-6'-methyl-5-nitro-4'-(3-nitro-phenyl)-2'-phenyl-1',4'-dihydro-[2,5']bipyrimidinyl
CAS No.:162851-32-3
Molecular Formula:C₂₃H₂₀N₆O₆
Molecular Weight:476.448
Hs Code.:

Synonyms:4,6-Dimethoxy-6'-methyl-5-nitro-4'-(3-nitro-phenyl)-2'-phenyl-1',4'-dihydro-[2,5']bipyrimidinyl

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Chemical Property of 4,6-Dimethoxy-6'-methyl-5-nitro-4'-(3-nitro-phenyl)-2'-phenyl-1',4'-dihydro-[2,5']bipyrimidinyl

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Technology Process of 4,6-Dimethoxy-6'-methyl-5-nitro-4'-(3-nitro-phenyl)-2'-phenyl-1',4'-dihydro-[2,5']bipyrimidinyl

There total 3 articles about 4,6-Dimethoxy-6'-methyl-5-nitro-4'-(3-nitro-phenyl)-2'-phenyl-1',4'-dihydro-[2,5']bipyrimidinyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 618-39-3
benzamidin

: (E)-3-(4,6-Dimethoxy-5-nitro-pyrimidin-2-yl)-4-(3-nitro-phenyl)-but-3-en-2-one

: 162851-32-3
4,6-Dimethoxy-6'-methyl-5-nitro-4'-(3-nitro-phenyl)-2'-phenyl-1',4'-dihydro-[2,5']bipyrimidinyl

Guidance literature:: With aluminum oxide; In benzene; for 6h; Heating;
DOI:10.1007/BF01169842

Reference yield:

: 99-61-6
3-nitro-benzaldehyde

: 162851-32-3
4,6-Dimethoxy-6'-methyl-5-nitro-4'-(3-nitro-phenyl)-2'-phenyl-1',4'-dihydro-[2,5']bipyrimidinyl

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / AcOH, piperidine / benzene / 6 h / Heating

2: 48 percent / Al₂O₃ / benzene / 6 h / Heating

With piperidine; aluminum oxide; acetic acid; In benzene;
DOI:10.1007/BF01169842

Reference yield:

: 69098-63-1
1-(4,6-dimethoxy-5-nitro-pyrimidin-2-yl)-propan-2-one

: 162851-32-3
4,6-Dimethoxy-6'-methyl-5-nitro-4'-(3-nitro-phenyl)-2'-phenyl-1',4'-dihydro-[2,5']bipyrimidinyl

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / AcOH, piperidine / benzene / 6 h / Heating

2: 48 percent / Al₂O₃ / benzene / 6 h / Heating

With piperidine; aluminum oxide; acetic acid; In benzene;
DOI:10.1007/BF01169842