Technology Process of 4-(4-butylphenyl)butyl bromide
There total 5 articles about 4-(4-butylphenyl)butyl bromide which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 83 percent / AlCl3 / 1,2-dichloro-ethane / 0.5 h / 13 °C
2: 87 percent / H2, H2SO4 / 10percent Pd/C / ethyl acetate / 2585.7 Torr
3: 5.68 percent / 1.0 M BH3*THF / tetrahydrofuran / 1 h / Ambient temperature
4: Ph3P, CBr4 / CH2Cl2 / 0.75 h
With
aluminium trichloride; borane-THF; carbon tetrabromide; sulfuric acid; hydrogen; triphenylphosphine;
palladium on activated charcoal;
In
tetrahydrofuran; dichloromethane; ethyl acetate; 1,2-dichloro-ethane;
DOI:10.1021/jm00158a021
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 87 percent / H2, H2SO4 / 10percent Pd/C / ethyl acetate / 2585.7 Torr
2: 5.68 percent / 1.0 M BH3*THF / tetrahydrofuran / 1 h / Ambient temperature
3: Ph3P, CBr4 / CH2Cl2 / 0.75 h
With
borane-THF; carbon tetrabromide; sulfuric acid; hydrogen; triphenylphosphine;
palladium on activated charcoal;
In
tetrahydrofuran; dichloromethane; ethyl acetate;
DOI:10.1021/jm00158a021
- Guidance literature:
-
With
carbon tetrabromide; triphenylphosphine;
In
dichloromethane;
for 0.75h;
Yield given;
DOI:10.1021/jm00158a021