C₅₃H₆₄N₆O₁₃

Base Information

Chemical Name:C₅₃H₆₄N₆O₁₃
CAS No.:1343407-38-4
Molecular Formula:C₅₃H₆₄N₆O₁₃
Molecular Weight:993.124
Hs Code.:

C<sub>53</sub>H<sub>64</sub>N<sub>6</sub>O<sub>13</sub>

Synonyms:C₅₃H₆₄N₆O₁₃

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Chemical Property of C₅₃H₆₄N₆O₁₃

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Technology Process of C₅₃H₆₄N₆O₁₃

There total 13 articles about C₅₃H₆₄N₆O₁₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 1343407-37-3
C₅₅H₆₆N₆O₁₄

: 1343407-38-4
C₅₃H₆₄N₆O₁₃

Guidance literature:: With potassium carbonate; In methanol; water; at 20 ℃; for 0.833333h;

Reference yield:

: C₁₅H₁₈N₂O₈

: 1343407-38-4
C₅₃H₆₄N₆O₁₃

Guidance literature:: Multi-step reaction with 7 steps

1.1: trichloroisocyanuric acid; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / dichloromethane / 0 °C

2.1: 2,6-dimethylpyridine / dichloromethane / 1 h / -45 - 40 °C / Inert atmosphere

3.1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; ethanol; water / Inert atmosphere

4.1: lithium borohydride; ethanol / tetrahydrofuran / 1 h / 15 - 25 °C / Cooling with ice

5.1: zinc; acetic acid / ethanol / 0.08 h / Reflux

6.1: triethylamine / tetrahydrofuran / 0.17 h / 0 °C

6.2: 20 - 65 °C

7.1: potassium carbonate / water; methanol / 0.83 h / 20 °C

With 2,6-dimethylpyridine; lithium borohydride; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; ethanol; trichloroisocyanuric acid; sodium carbonate; potassium carbonate; acetic acid; triethylamine; zinc; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; toluene; 3.1: Suzuki Coupling;

Reference yield:

: 1343407-32-8
C₁₆H₁₅F₃N₂O₁₀S

: 1343407-38-4
C₅₃H₆₄N₆O₁₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; ethanol; water / Inert atmosphere

2.1: lithium borohydride; ethanol / tetrahydrofuran / 1 h / 15 - 25 °C / Cooling with ice

3.1: zinc; acetic acid / ethanol / 0.08 h / Reflux

4.1: triethylamine / tetrahydrofuran / 0.17 h / 0 °C

4.2: 20 - 65 °C

5.1: potassium carbonate / water; methanol / 0.83 h / 20 °C

With lithium borohydride; ethanol; sodium carbonate; potassium carbonate; acetic acid; triethylamine; zinc; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; methanol; ethanol; water; toluene; 1.1: Suzuki Coupling;