2,6-bis(dimethylaminomethyl)phenyldibismuthane

Base Information

Chemical Name:2,6-bis(dimethylaminomethyl)phenyldibismuthane
CAS No.:882031-93-8
Molecular Formula:C₄₈H₇₆Bi₂N₈
Molecular Weight:1183.15
Hs Code.:

Synonyms:2,6-bis(dimethylaminomethyl)phenyldibismuthane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,6-bis(dimethylaminomethyl)phenyldibismuthane

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Technology Process of 2,6-bis(dimethylaminomethyl)phenyldibismuthane

There total 2 articles about 2,6-bis(dimethylaminomethyl)phenyldibismuthane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 882031-96-1
BiCl(C₆H₃(CH₂N(CH₃)2)2)2

: 882031-93-8
2,6-bis(dimethylaminomethyl)phenyldibismuthane

Guidance literature:: With magnesium; 1,2-dibromoethane; In tetrahydrofuran; under Ar atm. soln. Bi complex in THF was added at -20°C to Mg activated with 1,2-dibromoethane and stirred for 3 h, warmed to 10°C; solvent was removed in vacuo, residue was extd. with petroleum ether andfiltered, solvent was removed in vacuo;
DOI:10.1021/ic052160n

Reference yield:

: 19851-44-6
1,3-bis[(dimethylamino)methyl]benzene

: 882031-93-8
2,6-bis(dimethylaminomethyl)phenyldibismuthane

Guidance literature:: Multi-step reaction with 2 steps

1: butyllithium / diethyl ether

2: magnesium; 1,2-dibromoethane / tetrahydrofuran

With butyllithium; magnesium; 1,2-dibromoethane; In tetrahydrofuran; diethyl ether;
DOI:10.1021/ic052160n

Reference yield:

: 60-29-7,927820-24-4
diethyl ether

: 882031-93-8
2,6-bis(dimethylaminomethyl)phenyldibismuthane

: 882031-99-4
[2,6-(Me₂NCH₂)2C₆H₃]4Bi₂(O₂)*OEt₂

Guidance literature:: With air; In diethyl ether; slow access air to soln. Bi complex in Et2O at -28°C; recrystn. from Et2O;
DOI:10.1021/ic052160n