2-[3-(t-butoxycarbonylaminomethyl)-4-cyanophenylamino]-2-(5-ethyl-2-fluoro-3-triisopropylsilanyloxyphenyl)thioacetimidic acid methyl ester

Base Information

• Chemical Name: 2-[3-(t-butoxycarbonylaminomethyl)-4-cyanophenylamino]-2-(5-ethyl-2-fluoro-3-triisopropylsilanyloxyphenyl)thioacetimidic acid methyl ester
• CAS No.: 1134559-74-2
• Molecular Formula: C₃₃H₄₉FN₄O₃SSi
• Molecular Weight: 628.927

Synonyms:2-[3-(t-butoxycarbonylaminomethyl)-4-cyanophenylamino]-2-(5-ethyl-2-fluoro-3-triisopropylsilanyloxyphenyl)thioacetimidic acid methyl ester

Chemical Property of 2-[3-(t-butoxycarbonylaminomethyl)-4-cyanophenylamino]-2-(5-ethyl-2-fluoro-3-triisopropylsilanyloxyphenyl)thioacetimidic acid methyl ester

Chemical Property:

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Technology Process of 2-[3-(t-butoxycarbonylaminomethyl)-4-cyanophenylamino]-2-(5-ethyl-2-fluoro-3-triisopropylsilanyloxyphenyl)thioacetimidic acid methyl ester

There total 1 articles about 2-[3-(t-butoxycarbonylaminomethyl)-4-cyanophenylamino]-2-(5-ethyl-2-fluoro-3-triisopropylsilanyloxyphenyl)thioacetimidic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

[2-cyano-(5-{[(5-ethyl-2-fluoro-3-triisopropylsilanyloxy)phenyl]thiocarbamoylmethyl}amino)benzyl]carbamic acid t-butyl ester (1134559-70-8) + trimethoxonium tetrafluoroborate (420-37-1) → 2-[3-(t-butoxycarbonylaminomethyl)-4-cyanophenylamino]-2-(5-ethyl-2-fluoro-3-triisopropylsilanyloxyphenyl)thioacetimidic acid methyl ester (1134559-74-2)

Guidance literature:

In acetonitrile; at 20 ℃; for 3h;

Reference yield:

2-[3-(t-butoxycarbonylaminomethyl)-4-cyanophenylamino]-2-(5-ethyl-2-fluoro-3-triisopropylsilanyloxyphenyl)thioacetimidic acid methyl ester (1134559-74-2) → 2-[3-(t-butoxycarbonylaminomethyl)-4-cyanophenylimino]-2-(5-ethyl-2-fluoro-3-triisopropylsilanyloxyphenyl)thioacetimidic acid methyl ester (1134559-77-5)

Guidance literature:

With manganese(IV) oxide; In ethyl acetate; at 20 ℃; for 9h;

upstream raw materials:

[2-cyano-(5-{[(5-ethyl-2-fluoro-3-triisopropylsilanyloxy)phenyl]thiocarbamoylmethyl}amino)benzyl]carbamic acid t-butyl ester

trimethoxonium tetrafluoroborate

Downstream raw materials:

2-[3-(t-butoxycarbonylaminomethyl)-4-cyanophenylimino]-2-(5-ethyl-2-fluoro-3-triisopropylsilanyloxyphenyl)thioacetimidic acid methyl ester

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