Co(NC₅H₃(C(CH₃)NC₆H₁₁)2)Cl₂

Base Information

Chemical Name:Co(NC₅H₃(C(CH₃)NC₆H₁₁)2)Cl₂
CAS No.:21295-24-9
Molecular Formula:C₂₁H₃₁Cl₂CoN₃
Molecular Weight:455.396
Hs Code.:

Co(NC<sub>5</sub>H<sub>3</sub>(C(CH<sub>3</sub>)NC<sub>6</sub>H<sub>11</sub>)2)Cl<sub>2</sub>

Synonyms:Co(NC₅H₃(C(CH₃)NC₆H₁₁)2)Cl₂

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Chemical Property of Co(NC₅H₃(C(CH₃)NC₆H₁₁)2)Cl₂

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Technology Process of Co(NC₅H₃(C(CH₃)NC₆H₁₁)2)Cl₂

There total 1 articles about Co(NC₅H₃(C(CH₃)NC₆H₁₁)2)Cl₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 204856-92-8
2,6-bis[1-(cyclohexylphenylimino)ethyl]pyridine

: 7646-79-9,14543-09-0,16413-89-1
cobalt(II) chloride

: 21295-24-9
Co(NC₅H₃(C(CH₃)NC₆H₁₁)2)Cl₂

Guidance literature:: In tetrahydrofuran; THF added to mixt. of CoCl2 and ligand; stirred for 12 h; modified from R. N. Davis et al., Inorg. Chim. Acta, 2007, 360, 3061; filtered; ppt. washed with pentane;
DOI:10.1021/ic100717w

Reference yield: 74.0%

: 21295-24-9
Co(NC₅H₃(C(CH₃)NC₆H₁₁)2)Cl₂

: 917-54-4
methyllithium

: 1234351-63-3
(^CyAPDI)CoCH₃

Guidance literature:: In diethyl ether; at 20 ℃; for 2.16667h; Cooling with liquid nitrogen;
DOI:10.1021/jacs.7b00445

Reference yield: 63.0%

: 21295-24-9
Co(NC₅H₃(C(CH₃)NC₆H₁₁)2)Cl₂

: Co(NC₅H₃(C(CH₃)NC₆H₁₁)2)Cl

Guidance literature:: With NaEt₃BH; In toluene; toluene slurry of Co complex cooled in liq. N2; toluene soln. of NaEt3BHadded dropwise with stirring; warmed to ambient temp. with stirring; soln. filtered through Celite; concd.; cooled to -35°C; elem. anal.;
DOI:10.1021/ic100717w