C₆₃H₆₉N₃O₁₄Si

Base Information

Chemical Name:C₆₃H₆₉N₃O₁₄Si
CAS No.:1262887-50-2
Molecular Formula:C₆₃H₆₉N₃O₁₄Si
Molecular Weight:1120.34
Hs Code.:

C<sub>63</sub>H<sub>69</sub>N<sub>3</sub>O<sub>14</sub>Si

Synonyms:C₆₃H₆₉N₃O₁₄Si

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Chemical Property of C₆₃H₆₉N₃O₁₄Si

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Technology Process of C₆₃H₆₉N₃O₁₄Si

There total 16 articles about C₆₃H₆₉N₃O₁₄Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1262887-46-6
C₅₈H₆₃N₃O₁₂Si

: 40608-06-8
levulinic anhydride

: 1262887-50-2
C₆₃H₆₉N₃O₁₄Si

Guidance literature:: With dmap; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; at 10 - 20 ℃; for 16h; Inert atmosphere; Industry scale;

Reference yield:

: 55682-48-9
1,6-anhydro-2-azido-3,4-di-O-benzyl-2-deoxy-D-glucopyranose

: 1262887-50-2
C₆₃H₆₉N₃O₁₄Si

Guidance literature:: Multi-step reaction with 7 steps

1: boron trifluoride diethyl etherate / dichloromethane / 3 h / -10 - 20 °C / Industry scale; Inert atmosphere

2: hydrazinium monoacetate / N,N-dimethyl-formamide / 3 h / 20 °C / Industry scale

3: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 2 h / 20 °C / Inert atmosphere; Industry scale

4: triethylsilyl trifluoromethyl sulfonate / dichloromethane / 2 h / -40 °C / Industry scale; Inert atmosphere

5: trifluoroacetic acid / 4 h / -5 - 20 °C / Industry scale

6: 1H-imidazole / dichloromethane / -20 - 20 °C / Inert atmosphere; Industry scale

7: dmap; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 16 h / 10 - 20 °C / Inert atmosphere; Industry scale

With 1H-imidazole; dmap; boron trifluoride diethyl etherate; triethylsilyl trifluoromethyl sulfonate; hydrazinium monoacetate; 1,8-diazabicyclo[5.4.0]undec-7-ene; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 604-69-3
β-D-glucose pentaacetate

: 1262887-50-2
C₆₃H₆₉N₃O₁₄Si

Guidance literature:: Multi-step reaction with 12 steps

1.1: hydrogen bromide; acetic acid / dichloromethane / 3 h / 0 - 20 °C

2.1: tetra-(n-butyl)ammonium iodide; sodium tetrahydroborate / acetonitrile / 16 h / 40 °C / Molecular sieve

3.1: sodium methylate / methanol / 3 h / 50 °C

4.1: (1S)-10-camphorsulfonic acid / 2 h / 50 °C

5.1: sodium hydride / tetrahydrofuran / 0.5 h / 0 °C

5.2: 0.5 h

6.1: trifluoroacetic acid; water / dichloromethane / 0 °C

7.1: tetrabutyl-ammonium chloride; sodium hydrogencarbonate; sodium hypochlorite; sodium bromide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / ethyl acetate / 16 h / 20 °C

8.1: triethylamine; dicyclohexyl-carbodiimide; benzotriazol-1-ol / dichloromethane / 16 h / 20 °C

9.1: triethylsilyl trifluoromethyl sulfonate / dichloromethane / 2 h / -40 °C / Industry scale; Inert atmosphere

10.1: trifluoroacetic acid / 4 h / -5 - 20 °C / Industry scale

11.1: 1H-imidazole / dichloromethane / -20 - 20 °C / Inert atmosphere; Industry scale

12.1: dmap; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 16 h / 10 - 20 °C / Inert atmosphere; Industry scale

With 1H-imidazole; dmap; sodium hypochlorite; sodium tetrahydroborate; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; (1S)-10-camphorsulfonic acid; tetrabutyl-ammonium chloride; water; hydrogen bromide; triethylsilyl trifluoromethyl sulfonate; sodium methylate; tetra-(n-butyl)ammonium iodide; sodium hydride; sodium hydrogencarbonate; benzotriazol-1-ol; acetic acid; triethylamine; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; trifluoroacetic acid; sodium bromide; In tetrahydrofuran; methanol; dichloromethane; ethyl acetate; acetonitrile;