trans-11,12-Bis(diphenylphosphinoxymethyl)-9,10-dihydro-9,10-ethanoanthracen

Base Information

Chemical Name:trans-11,12-Bis(diphenylphosphinoxymethyl)-9,10-dihydro-9,10-ethanoanthracen
CAS No.:134920-70-0
Molecular Formula:C₄₂H₃₆O₂P₂
Molecular Weight:634.694
Hs Code.:

Synonyms:trans-11,12-Bis(diphenylphosphinoxymethyl)-9,10-dihydro-9,10-ethanoanthracen

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Chemical Property of trans-11,12-Bis(diphenylphosphinoxymethyl)-9,10-dihydro-9,10-ethanoanthracen

Chemical Property:

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Technology Process of trans-11,12-Bis(diphenylphosphinoxymethyl)-9,10-dihydro-9,10-ethanoanthracen

There total 3 articles about trans-11,12-Bis(diphenylphosphinoxymethyl)-9,10-dihydro-9,10-ethanoanthracen which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 71991-70-3
trans-11,12-Bis(dihydroxymethyl)-9,10-dihydro-9,10-ethanoanthracen

: 1079-66-9,74391-44-9
chloro-diphenylphosphine

: 134920-70-0
trans-11,12-Bis(diphenylphosphinoxymethyl)-9,10-dihydro-9,10-ethanoanthracen

Guidance literature:: With pyridine; In tetrahydrofuran; at 20 ℃; for 4h;

Reference yield:

: 27069-21-2
trans-9,10-dihydro-9,10-ethanoanthracene-11,12-dicarboxylic acid

: 134920-70-0
trans-11,12-Bis(diphenylphosphinoxymethyl)-9,10-dihydro-9,10-ethanoanthracen

Guidance literature:: Multi-step reaction with 2 steps

1: 72 percent / LiAlH₄ / diethyl ether / 1 h / Heating

2: 57 percent / pyridine / tetrahydrofuran / 4 h / 20 °C

With pyridine; lithium aluminium tetrahydride; In tetrahydrofuran; diethyl ether;

Reference yield:

: 33741-21-8
9,10-Dihydro-9,10-ethano-11,12-trans-dicarbonsaeure dimethylester

: 134920-70-0
trans-11,12-Bis(diphenylphosphinoxymethyl)-9,10-dihydro-9,10-ethanoanthracen

Guidance literature:: Multi-step reaction with 2 steps

1: 72 percent / LiAlH₄ / diethyl ether / 1 h / Heating

2: 57 percent / pyridine / tetrahydrofuran / 4 h / 20 °C

With pyridine; lithium aluminium tetrahydride; In tetrahydrofuran; diethyl ether;