(2S)-2-(3-(tert-butoxycarbonylamino)propyl)-3-formyl-1-(toluene-4-sulfonyl)-1,2-dihydroquinoline-6-carboxylc acid methyl ester

Base Information

Chemical Name:(2S)-2-(3-(tert-butoxycarbonylamino)propyl)-3-formyl-1-(toluene-4-sulfonyl)-1,2-dihydroquinoline-6-carboxylc acid methyl ester
CAS No.:1100289-42-6
Molecular Formula:C₂₇H₃₂N₂O₇S
Molecular Weight:528.626
Hs Code.:

Synonyms:(2S)-2-(3-(tert-butoxycarbonylamino)propyl)-3-formyl-1-(toluene-4-sulfonyl)-1,2-dihydroquinoline-6-carboxylc acid methyl ester

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Chemical Property of (2S)-2-(3-(tert-butoxycarbonylamino)propyl)-3-formyl-1-(toluene-4-sulfonyl)-1,2-dihydroquinoline-6-carboxylc acid methyl ester

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Technology Process of (2S)-2-(3-(tert-butoxycarbonylamino)propyl)-3-formyl-1-(toluene-4-sulfonyl)-1,2-dihydroquinoline-6-carboxylc acid methyl ester

There total 2 articles about (2S)-2-(3-(tert-butoxycarbonylamino)propyl)-3-formyl-1-(toluene-4-sulfonyl)-1,2-dihydroquinoline-6-carboxylc acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 760968-76-1
tert-butyl (6-oxohex-4-enyl)carbamate

: 1100289-40-4
3-formyl-4-(toluene-4-sulfonylamino)-benzoic acid methyl ester

: 1100289-42-6
(2S)-2-(3-(tert-butoxycarbonylamino)propyl)-3-formyl-1-(toluene-4-sulfonyl)-1,2-dihydroquinoline-6-carboxylc acid methyl ester

Guidance literature:: With (R)-diphenylprolinol triethylsilyl ether; In acetonitrile; at -20 ℃; for 24h; optical yield given as %ee;
DOI:10.1016/j.tet.2008.10.032

Reference yield:

: 760968-76-1
tert-butyl (6-oxohex-4-enyl)carbamate

: 1100289-40-4
3-formyl-4-(toluene-4-sulfonylamino)-benzoic acid methyl ester

: (2R)-2-(3-(tert-butoxycarbonylamino)propyl)-3-formyl-1-(toluene-4-sulfonyl)-1,2-dihydroquinoline-6-carboxylc acid methyl ester

: 1100289-42-6
(2S)-2-(3-(tert-butoxycarbonylamino)propyl)-3-formyl-1-(toluene-4-sulfonyl)-1,2-dihydroquinoline-6-carboxylc acid methyl ester

Guidance literature:: With (S)-2-(diphenyl((triethylsilyl)oxy)methyl)pyrrolidine; sodium acetate; In acetonitrile; at 20 ℃; for 43.5h; optical yield given as %ee;
DOI:10.1016/j.tet.2008.10.032