methyl 3-N'-(4'-trifluoromethylbenzoyl)hydrazino-2,2,5-trimethylhexanoate

Base Information

• Chemical Name: methyl 3-N'-(4'-trifluoromethylbenzoyl)hydrazino-2,2,5-trimethylhexanoate
• CAS No.: 215536-63-3
• Molecular Formula: C₁₈H₂₅F₃N₂O₃
• Molecular Weight: 374.403
• Mol file: 215536-63-3.mol

Synonyms:methyl 3-N'-(4'-trifluoromethylbenzoyl)hydrazino-2,2,5-trimethylhexanoate

Chemical Property of methyl 3-N'-(4'-trifluoromethylbenzoyl)hydrazino-2,2,5-trimethylhexanoate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of methyl 3-N'-(4'-trifluoromethylbenzoyl)hydrazino-2,2,5-trimethylhexanoate

There total 1 articles about methyl 3-N'-(4'-trifluoromethylbenzoyl)hydrazino-2,2,5-trimethylhexanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

1-methoxy-2-methyl-1-trimethylsiloxy-1-propene (31469-15-5) + isovaleraldehyde 4-trifluoromethylbenzoylhydrazone → methyl 3-N'-(4'-trifluoromethylbenzoyl)hydrazino-2,2,5-trimethylhexanoate (215536-63-3)

Guidance literature:

With scandium tris(trifluoromethanesulfonate); In acetonitrile; for 4h; Ambient temperature;

DOI:10.1055/s-1998-1843

Reference yield: 93.0%

methyl 3-N'-(4'-trifluoromethylbenzoyl)hydrazino-2,2,5-trimethylhexanoate (215536-63-3) → 4-isobutyl-3,3-dimethyl-1-(4'-trifluoromethylbenzoyl)aminoazetidin-2-one

Guidance literature:

With n-butyllithium; at -78 ℃;

DOI:10.1055/s-1998-1843

upstream raw materials:

1-methoxy-2-methyl-1-trimethylsiloxy-1-propene