1-Benzyl-6-[1-(6-methoxy-7-methyl-benzo[1,3]dioxol-5-yl)-meth-(Z)-ylidene]-3-(2,4,5-trimethoxy-3-methyl-benzyl)-piperazine-2,5-dione

Base Information

Chemical Name:1-Benzyl-6-[1-(6-methoxy-7-methyl-benzo[1,3]dioxol-5-yl)-meth-(Z)-ylidene]-3-(2,4,5-trimethoxy-3-methyl-benzyl)-piperazine-2,5-dione
CAS No.:187040-27-3
Molecular Formula:C₃₂H₃₄N₂O₈
Molecular Weight:574.631
Hs Code.:

Synonyms:1-Benzyl-6-[1-(6-methoxy-7-methyl-benzo[1,3]dioxol-5-yl)-meth-(Z)-ylidene]-3-(2,4,5-trimethoxy-3-methyl-benzyl)-piperazine-2,5-dione

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Chemical Property of 1-Benzyl-6-[1-(6-methoxy-7-methyl-benzo[1,3]dioxol-5-yl)-meth-(Z)-ylidene]-3-(2,4,5-trimethoxy-3-methyl-benzyl)-piperazine-2,5-dione

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Technology Process of 1-Benzyl-6-[1-(6-methoxy-7-methyl-benzo[1,3]dioxol-5-yl)-meth-(Z)-ylidene]-3-(2,4,5-trimethoxy-3-methyl-benzyl)-piperazine-2,5-dione

There total 11 articles about 1-Benzyl-6-[1-(6-methoxy-7-methyl-benzo[1,3]dioxol-5-yl)-meth-(Z)-ylidene]-3-(2,4,5-trimethoxy-3-methyl-benzyl)-piperazine-2,5-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 187040-26-2
1-Acetyl-4-benzyl-3-[1-(6-methoxy-7-methyl-benzo[1,3]dioxol-5-yl)-meth-(Z)-ylidene]-6-(2,4,5-trimethoxy-3-methyl-benzyl)-piperazine-2,5-dione

: 187040-27-3
1-Benzyl-6-[1-(6-methoxy-7-methyl-benzo[1,3]dioxol-5-yl)-meth-(Z)-ylidene]-3-(2,4,5-trimethoxy-3-methyl-benzyl)-piperazine-2,5-dione

Guidance literature:: With hydrazine hydrate; In N,N-dimethyl-formamide; for 1h; Yield given; Ambient temperature;

Reference yield:

: 80592-18-3
3,4-methylenedioxyphenyl formate

: 187040-27-3
1-Benzyl-6-[1-(6-methoxy-7-methyl-benzo[1,3]dioxol-5-yl)-meth-(Z)-ylidene]-3-(2,4,5-trimethoxy-3-methyl-benzyl)-piperazine-2,5-dione

Guidance literature:: Multi-step reaction with 9 steps

1: 10percent aq. KOH / methanol / 2.5 h / Ambient temperature

2: 99 percent / NaH / dimethylformamide / 1.) 0 deg C, 30 min, 2.) 0 deg C, 3 h

3: 72 percent / BuLi / tetrahydrofuran / 1.) -17 deg C, 1 h, 2.) -17 deg C, 2 h

4: 77 percent / conc. aq. HCl / ethanol / 3 h / Heating

5: 73 percent / acetic acid / 0.5 h / Heating

6: 80 percent / NaH / dimethylformamide / 1.) 0 deg C, 30 min, 2.) 0 deg C, 1 h

7: 74 percent / t-BuOK / 2-methyl-propan-2-ol; dimethylformamide / 24 h / Ambient temperature

8: NaH / dimethylformamide / 1.) 0 deg C, 30 min, 2.) r.t., 2 h

9: NH₂NH₂*H₂O / dimethylformamide / 1 h / Ambient temperature

With hydrogenchloride; potassium hydroxide; n-butyllithium; potassium tert-butylate; sodium hydride; hydrazine hydrate; In tetrahydrofuran; methanol; ethanol; acetic acid; N,N-dimethyl-formamide; tert-butyl alcohol;

Reference yield:

: 533-31-3
Sesamol

: 187040-27-3
1-Benzyl-6-[1-(6-methoxy-7-methyl-benzo[1,3]dioxol-5-yl)-meth-(Z)-ylidene]-3-(2,4,5-trimethoxy-3-methyl-benzyl)-piperazine-2,5-dione

Guidance literature:: Multi-step reaction with 8 steps

1: 99 percent / NaH / dimethylformamide / 1.) 0 deg C, 30 min, 2.) 0 deg C, 3 h

2: 72 percent / BuLi / tetrahydrofuran / 1.) -17 deg C, 1 h, 2.) -17 deg C, 2 h

3: 77 percent / conc. aq. HCl / ethanol / 3 h / Heating

4: 73 percent / acetic acid / 0.5 h / Heating

5: 80 percent / NaH / dimethylformamide / 1.) 0 deg C, 30 min, 2.) 0 deg C, 1 h

6: 74 percent / t-BuOK / 2-methyl-propan-2-ol; dimethylformamide / 24 h / Ambient temperature

7: NaH / dimethylformamide / 1.) 0 deg C, 30 min, 2.) r.t., 2 h

8: NH₂NH₂*H₂O / dimethylformamide / 1 h / Ambient temperature

With hydrogenchloride; n-butyllithium; potassium tert-butylate; sodium hydride; hydrazine hydrate; In tetrahydrofuran; ethanol; acetic acid; N,N-dimethyl-formamide; tert-butyl alcohol;