anti-9-<1-(p-chlorophenyl)>-cis-bicyclo<6.1.0>nona-2,4,6-triene

Base Information

• Chemical Name: anti-9-<1-(p-chlorophenyl)>-cis-bicyclo<6.1.0>nona-2,4,6-triene
• CAS No.: 96395-03-8
• Molecular Formula: C₁₅H₁₃Cl
• Molecular Weight: 228.721
• Mol file: 96395-03-8.mol

Synonyms:anti-9-<1-(p-chlorophenyl)>-cis-bicyclo<6.1.0>nona-2,4,6-triene

Chemical Property of anti-9-<1-(p-chlorophenyl)>-cis-bicyclo<6.1.0>nona-2,4,6-triene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of anti-9-<1-(p-chlorophenyl)>-cis-bicyclo<6.1.0>nona-2,4,6-triene

There total 1 articles about anti-9-<1-(p-chlorophenyl)>-cis-bicyclo<6.1.0>nona-2,4,6-triene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

1,3,5,7-cyclooctatetraene (629-20-9) + (4-chlorophenyl)dichloromethane (13940-94-8) → anti-9-<1-(p-chlorophenyl)>-cis-bicyclo<6.1.0>nona-2,4,6-triene (96395-03-8)

Guidance literature:

With lithium; In diethyl ether; ammonia; at -33 ℃; for 1h;

DOI:10.1021/ja00299a039

Reference yield:

anti-9-<1-(p-chlorophenyl)>-cis-bicyclo<6.1.0>nona-2,4,6-triene (96395-03-8) → 9-<1-(p-chlorophenyl)>methylenecyclooctatrienyl lithium (78585-74-7)

Guidance literature:

With lithium amide; In ammonia; at -60 ℃;

DOI:10.1021/ja00299a039

upstream raw materials:

1,3,5,7-cyclooctatetraene

(4-chlorophenyl)dichloromethane

Downstream raw materials:

9-<1-(p-chlorophenyl)>methylenecyclooctatrienyl lithium