(2'R,3'S)-methyl 2-[3-(benzyloxycarbonylamino)-2-hydroxybutyl]propenoate

Base Information

• Chemical Name: (2'R,3'S)-methyl 2-[3-(benzyloxycarbonylamino)-2-hydroxybutyl]propenoate
• CAS No.: 241149-73-5
• Molecular Formula: C₁₆H₂₁NO₅
• Molecular Weight: 307.346

Synonyms:(2'R,3'S)-methyl 2-[3-(benzyloxycarbonylamino)-2-hydroxybutyl]propenoate

Chemical Property of (2'R,3'S)-methyl 2-[3-(benzyloxycarbonylamino)-2-hydroxybutyl]propenoate

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Technology Process of (2'R,3'S)-methyl 2-[3-(benzyloxycarbonylamino)-2-hydroxybutyl]propenoate

There total 10 articles about (2'R,3'S)-methyl 2-[3-(benzyloxycarbonylamino)-2-hydroxybutyl]propenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

methyl 2-(bromomethyl)propenoate (4224-69-5) + (2S,3S)-3-methyl-1-oxopentane-2-benzylcarbamate (149357-59-5) → (2'R,3'S)-methyl 2-[3-(benzyloxycarbonylamino)-2-hydroxybutyl]propenoate (241149-73-5) + (2'S,3'S,4'S)-methyl 2-[3-(benzyloxycarbonylamino)-2-hydroxy-4-methylhexyl]propenoate (241149-82-6)

Guidance literature:

With indium; water; In ethanol; at 20 ℃; for 4h;

DOI:10.1002/(sici)1099-0690(199907)1999:7<1551::aid-ejoc1551>3.0.co;2-8

Reference yield: 68.0%

methyl 2-(bromomethyl)propenoate (4224-69-5) + N-benzyloxycarbonyl-L-valinal (138754-84-4,95500-73-5) → (2'R,3'S)-methyl 2-[3-(benzyloxycarbonylamino)-2-hydroxybutyl]propenoate (241149-73-5) + (2'S,3'S)-methyl 2-[3-(benzyloxycarbonylamino)-2-hydroxy-4-methylpentyl]propenoate (241149-80-4)

Guidance literature:

With indium; water; In ethanol; at 20 ℃; for 4h;

DOI:10.1002/(sici)1099-0690(199907)1999:7<1551::aid-ejoc1551>3.0.co;2-8

Reference yield: 60.0%

methyl 2-(bromomethyl)propenoate (4224-69-5) + N-carbobenzoxy-L-leucinal (70853-26-8,86852-22-4,71413-15-5) → (2'R,3'S)-methyl 2-[3-(benzyloxycarbonylamino)-2-hydroxybutyl]propenoate (241149-73-5) + (2'S,3'S)-methyl 2-[3-(benzyloxycarbonylamino)-2-hydroxy-5-methylhexyl]propenoate (241149-78-0)

Guidance literature:

With indium; water; In ethanol; at 20 ℃; for 4h;

DOI:10.1002/(sici)1099-0690(199907)1999:7<1551::aid-ejoc1551>3.0.co;2-8

upstream raw materials:

methyl 2-(bromomethyl)propenoate

benzyl (S)-1-oxopropan-2-ylcarbamate

N-carbobenzoxy-L-leucinal

benzyl (1S)-(1-formyl-2-phenylethyl)carbamate

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