Technology Process of isoflavan-5,7-diol
There total 4 articles about isoflavan-5,7-diol which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydrogen;
palladium on activated charcoal;
In
acetic acid; ethyl acetate;
for 6h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1.) POCl3, 2.) NaBF4 / 1.) 20 deg C to 70 deg C, 7.5 h, 2.) 1 h
2: 10.3 g / 25percent aq. NaOH / ethanol / 3 h / Heating
3: 3.8 g / 36percent HCl / acetic acid / 4 h
4: 0.44 g / H2 / 5percent Pd/C / acetic acid; ethyl acetate / 6 h
With
hydrogenchloride; sodium hydroxide; sodium tetrafluoroborate; hydrogen; trichlorophosphate;
palladium on activated charcoal;
In
ethanol; acetic acid; ethyl acetate;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 10.3 g / 25percent aq. NaOH / ethanol / 3 h / Heating
2: 3.8 g / 36percent HCl / acetic acid / 4 h
3: 0.44 g / H2 / 5percent Pd/C / acetic acid; ethyl acetate / 6 h
With
hydrogenchloride; sodium hydroxide; hydrogen;
palladium on activated charcoal;
In
ethanol; acetic acid; ethyl acetate;