(R)-4-O-tert-butyldimethylsilyl-1'-hydroxychavicol

Base Information

Chemical Name:(R)-4-O-tert-butyldimethylsilyl-1'-hydroxychavicol
CAS No.:387351-57-7
Molecular Formula:C₁₅H₂₄O₂Si
Molecular Weight:264.44
Hs Code.:

Synonyms:(R)-4-O-tert-butyldimethylsilyl-1'-hydroxychavicol

Suppliers and Price of (R)-4-O-tert-butyldimethylsilyl-1'-hydroxychavicol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R)-4-O-tert-butyldimethylsilyl-1'-hydroxychavicol

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Technology Process of (R)-4-O-tert-butyldimethylsilyl-1'-hydroxychavicol

There total 6 articles about (R)-4-O-tert-butyldimethylsilyl-1'-hydroxychavicol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 905266-48-0
1-(4-(tert-butyldimethylsilyloxy)phenyl)prop-2-en-1-one

: 387351-57-7
(R)-4-O-tert-butyldimethylsilyl-1'-hydroxychavicol

Guidance literature:: With dimethylsulfide borane complex; (S)-oxazaborolidine; In tetrahydrofuran; at -40 ℃; optical yield given as %ee;
DOI:10.1016/j.bmcl.2009.03.047

Reference yield:

: 387351-56-6
acetic acid 1-[4-(tert-butyl-dimethyl-silanyloxy)-phenyl]-allyl ester

: 387351-57-7
(R)-4-O-tert-butyldimethylsilyl-1'-hydroxychavicol

Guidance literature:: With phosphate buffer; Pseudomonas cepacia lipase PS; at 20 ℃; for 20h; pH=7.0;
DOI:10.1016/j.bmc.2005.10.029

Reference yield:

: 194156-04-2
1-(4-((tert-butyldimethylsilyl)oxy)phenyl)prop-2-en-1-ol

: 387351-57-7
(R)-4-O-tert-butyldimethylsilyl-1'-hydroxychavicol

Guidance literature:: Multi-step reaction with 2 steps

1: 50 percent / Pseudomonas cepacia lipase PS; 2,6-di-t-butyl-p-cresol / tetrahydrofuran / 24 h / 65 °C

2: 420 mg / Pseudomonas cepacia lipase PS; aq. phosphate buffer / 20 h / 20 °C / pH 7.0

With phosphate buffer; 2,6-di-tert-butyl-4-methyl-phenol; Pseudomonas cepacia lipase PS; In tetrahydrofuran;
DOI:10.1016/j.bmc.2005.10.029