1-(2,5-dimethoxyphenyl)-2-(isopropylamino)ethanol hydrochloride

Base Information

Chemical Name:1-(2,5-dimethoxyphenyl)-2-(isopropylamino)ethanol hydrochloride
CAS No.:83436-85-5
Molecular Formula:C₁₃H₂₁NO₃*ClH
Molecular Weight:275.776
Hs Code.:

Synonyms:1-(2,5-dimethoxyphenyl)-2-(isopropylamino)ethanol hydrochloride

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Chemical Property of 1-(2,5-dimethoxyphenyl)-2-(isopropylamino)ethanol hydrochloride

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Technology Process of 1-(2,5-dimethoxyphenyl)-2-(isopropylamino)ethanol hydrochloride

There total 3 articles about 1-(2,5-dimethoxyphenyl)-2-(isopropylamino)ethanol hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 83436-63-9
2-(Benzyl-isopropyl-amino)-1-(2,5-dimethoxy-phenyl)-ethanol; hydrochloride

: 83436-85-5
1-(2,5-dimethoxyphenyl)-2-(isopropylamino)ethanol hydrochloride

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; at 50 ℃; under 760 Torr;
DOI:10.1021/jm00356a026

Reference yield:

: 1204-21-3
2-bromo-2',5'-dimethoxyacetophenone

: 83436-85-5
1-(2,5-dimethoxyphenyl)-2-(isopropylamino)ethanol hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: 82 percent / diethyl ether / 5 h / Ambient temperature

2: 44 percent / NaBH₄, 2 N aq. NaOH / methanol / 1 h / Ambient temperature

3: 45 percent / H₂ / 10percent Pd/C / ethanol / 50 °C / 760 Torr

With sodium hydroxide; sodium tetrahydroborate; hydrogen; palladium on activated charcoal; In methanol; diethyl ether; ethanol;
DOI:10.1021/jm00356a026

Reference yield:

: 83436-59-3
2,5-dimethoxy-ω-(N-benzyl-N-isopropylamino)acetophenone hydrochloride

: 83436-85-5
1-(2,5-dimethoxyphenyl)-2-(isopropylamino)ethanol hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 44 percent / NaBH₄, 2 N aq. NaOH / methanol / 1 h / Ambient temperature

2: 45 percent / H₂ / 10percent Pd/C / ethanol / 50 °C / 760 Torr

With sodium hydroxide; sodium tetrahydroborate; hydrogen; palladium on activated charcoal; In methanol; ethanol;
DOI:10.1021/jm00356a026