methyl 3-<(2S,3R)-3-(benzyloxy)-3,4,5,6-tetrahydro-2H-pyran-2-yl>propanoate

Base Information

Chemical Name:methyl 3-<(2S,3R)-3-(benzyloxy)-3,4,5,6-tetrahydro-2H-pyran-2-yl>propanoate
CAS No.:125877-79-4
Molecular Formula:C₁₆H₂₂O₄
Molecular Weight:278.348
Hs Code.:

Synonyms:methyl 3-<(2S,3R)-3-(benzyloxy)-3,4,5,6-tetrahydro-2H-pyran-2-yl>propanoate

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Chemical Property of methyl 3-<(2S,3R)-3-(benzyloxy)-3,4,5,6-tetrahydro-2H-pyran-2-yl>propanoate

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Technology Process of methyl 3-<(2S,3R)-3-(benzyloxy)-3,4,5,6-tetrahydro-2H-pyran-2-yl>propanoate

There total 5 articles about methyl 3-<(2S,3R)-3-(benzyloxy)-3,4,5,6-tetrahydro-2H-pyran-2-yl>propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 125901-89-5
methyl (E)-3-<(2S,3R)-3-(benzyloxy)-3,4,5,6-tetrahydro-2H-pyran-2-yl>propenoate

: 125877-79-4
methyl 3-<(2S,3R)-3-(benzyloxy)-3,4,5,6-tetrahydro-2H-pyran-2-yl>propanoate

Guidance literature:: With hydrogen; palladium on activated charcoal; In hexane; for 3h; Ambient temperature;
DOI:10.1021/ja00164a026

Reference yield:

: 121422-51-3
(2S,3R)-3-hydroxy-2-vinyloxane

: 125877-79-4
methyl 3-<(2S,3R)-3-(benzyloxy)-3,4,5,6-tetrahydro-2H-pyran-2-yl>propanoate

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) KH / 1.) THF, 0 deg C, 10 min, 2.) 25 deg C, 3 h

2: 1.) ozone, 2.) Me₂S / 1.) CH₂Cl₂, -78 deg C, 0.5 h, 2.) from -78 deg C to RT, 1 h

3: benzene / 3 h / Ambient temperature

4: 100 percent / H₂ / 5percent Pd/C / hexane / 3 h / Ambient temperature

With dimethylsulfide; hydrogen; potassium hydride; ozone; palladium on activated charcoal; In hexane; benzene;
DOI:10.1021/ja00164a026

Reference yield:

: 125877-78-3
(2R,3R)-3-Benzyloxy-tetrahydro-pyran-2-carbaldehyde

: 125877-79-4
methyl 3-<(2S,3R)-3-(benzyloxy)-3,4,5,6-tetrahydro-2H-pyran-2-yl>propanoate

Guidance literature:: Multi-step reaction with 2 steps

1: benzene / 3 h / Ambient temperature

2: 100 percent / H₂ / 5percent Pd/C / hexane / 3 h / Ambient temperature

With hydrogen; palladium on activated charcoal; In hexane; benzene;
DOI:10.1021/ja00164a026