3-{4-amino-3-[3-(3-tert-butylphenylcarbamoyl)phenyl]pyrazolo[3,4-d]pyrimidin-1-yl}piperidinium chloride

Base Information

Chemical Name:3-{4-amino-3-[3-(3-tert-butylphenylcarbamoyl)phenyl]pyrazolo[3,4-d]pyrimidin-1-yl}piperidinium chloride
CAS No.:1407967-18-3
Molecular Formula:C₂₇H₃₁N₇O*ClH
Molecular Weight:506.05
Hs Code.:

Synonyms:3-{4-amino-3-[3-(3-tert-butylphenylcarbamoyl)phenyl]pyrazolo[3,4-d]pyrimidin-1-yl}piperidinium chloride

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Chemical Property of 3-{4-amino-3-[3-(3-tert-butylphenylcarbamoyl)phenyl]pyrazolo[3,4-d]pyrimidin-1-yl}piperidinium chloride

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Technology Process of 3-{4-amino-3-[3-(3-tert-butylphenylcarbamoyl)phenyl]pyrazolo[3,4-d]pyrimidin-1-yl}piperidinium chloride

There total 3 articles about 3-{4-amino-3-[3-(3-tert-butylphenylcarbamoyl)phenyl]pyrazolo[3,4-d]pyrimidin-1-yl}piperidinium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1407967-15-0
3-{4-amino-3-[3-(3-tert-butylphenylcarbamoyl)phenyl]pyrazolo[3,4-d]pyrimidin-1-yl}piperidine-1-carboxylic acid tert-butyl ester

: 1407967-18-3
3-{4-amino-3-[3-(3-tert-butylphenylcarbamoyl)phenyl]pyrazolo[3,4-d]pyrimidin-1-yl}piperidinium chloride

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; for 0.5h; Reflux;
DOI:10.1021/jm301190s

Reference yield:

: 1407967-12-7
3-[4-amino-3-(3-carboxyphenyl)pyrazolo[3,4-d]pyrimidin-1-yl]piperidine-1-carboxylicacid tert-butyl ester

: 1407967-18-3
3-{4-amino-3-[3-(3-tert-butylphenylcarbamoyl)phenyl]pyrazolo[3,4-d]pyrimidin-1-yl}piperidinium chloride

Guidance literature:: Multi-step reaction with 2 steps

1.1: 1,1'-carbonyldiimidazole / dichloromethane / 0.5 h

1.2: 0.5 h

2.1: hydrogenchloride / 1,4-dioxane / 0.5 h / Reflux

With hydrogenchloride; 1,1'-carbonyldiimidazole; In 1,4-dioxane; dichloromethane;
DOI:10.1021/jm301190s

Reference yield:

: 5369-19-7
3-tert-butylaniline

: 1407967-18-3
3-{4-amino-3-[3-(3-tert-butylphenylcarbamoyl)phenyl]pyrazolo[3,4-d]pyrimidin-1-yl}piperidinium chloride

Guidance literature:: Multi-step reaction with 2 steps

1.1: 1,1'-carbonyldiimidazole / dichloromethane / 0.5 h

1.2: 0.5 h

2.1: hydrogenchloride / 1,4-dioxane / 0.5 h / Reflux

With hydrogenchloride; 1,1'-carbonyldiimidazole; In 1,4-dioxane; dichloromethane;
DOI:10.1021/jm301190s