3'-<(Z)-2-(tert-Butoxycarbonylamino)-2-(methoxycarbonyl)vinyl>-4,4'-dibenzyloxy-3-(1,3-dioxan-2-yl)biphenyl

Base Information

• Chemical Name: 3'-<(Z)-2-(tert-Butoxycarbonylamino)-2-(methoxycarbonyl)vinyl>-4,4'-dibenzyloxy-3-(1,3-dioxan-2-yl)biphenyl
• CAS No.: 134038-81-6
• Molecular Formula: C₃₉H₄₁NO₈
• Molecular Weight: 651.756

Synonyms:3'-<(Z)-2-(tert-Butoxycarbonylamino)-2-(methoxycarbonyl)vinyl>-4,4'-dibenzyloxy-3-(1,3-dioxan-2-yl)biphenyl

Chemical Property of 3'-<(Z)-2-(tert-Butoxycarbonylamino)-2-(methoxycarbonyl)vinyl>-4,4'-dibenzyloxy-3-(1,3-dioxan-2-yl)biphenyl

Chemical Property:

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MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3'-<(Z)-2-(tert-Butoxycarbonylamino)-2-(methoxycarbonyl)vinyl>-4,4'-dibenzyloxy-3-(1,3-dioxan-2-yl)biphenyl

There total 19 articles about 3'-<(Z)-2-(tert-Butoxycarbonylamino)-2-(methoxycarbonyl)vinyl>-4,4'-dibenzyloxy-3-(1,3-dioxan-2-yl)biphenyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

4,4'-Dibenzyloxy-3-(1,3-dioxane-2-yl)biphenyl-3'-carbaldehyde (134038-80-5) + trimethyl 2-(tert-butoxycarbonylamino)phosphonoacetate (121056-95-9,89524-98-1) → 3'-<(Z)-2-(tert-Butoxycarbonylamino)-2-(methoxycarbonyl)vinyl>-4,4'-dibenzyloxy-3-(1,3-dioxan-2-yl)biphenyl (134038-81-6)

Guidance literature:

With 1,1,3,3-tetramethylguanidine; In tetrahydrofuran; 1) -70 deg C to r.t., overnight, 2) r.t., 1 d;

DOI:10.1055/s-1992-26293

Reference yield: 99.0%

4,4'-Dibenzyloxy-3-(1,3-dioxane-2-yl)biphenyl-3'-carbaldehyde (134038-80-5) + trimethyl 2-(tert-butoxycarbonylamino)phosphonoacetate (121056-95-9,89524-98-1) → (Z)-3-(4,4'-Bis-benzyloxy-3'-[1,3]dioxan-2-yl-biphenyl-3-yl)-2-tert-butoxycarbonylamino-acrylic acid methyl ester (134038-81-6,134038-90-7)

Guidance literature:

With 1,8-diazabicyclo[5.4.0]undec-7-ene; lithium chloride; In acetonitrile; for 1h; Ambient temperature;

DOI:10.1039/c39910000275

Reference yield: 95.0%

(Z)-3-(4,4'-Bis-benzyloxy-3'-[1,3]dioxan-2-yl-biphenyl-3-yl)-2-tert-butoxycarbonylamino-acrylic acid methyl ester (134038-81-6,134038-90-7) → 3'-<(Z)-2-(tert-Butoxycarbonylamino)-2-(methoxycarbonyl)vinyl>-4,4'-dibenzyloxy-3-(1,3-dioxan-2-yl)biphenyl (134038-81-6)

Guidance literature:

With NEt₃/C; In ethanol; chloroform; for 48h; Ambient temperature;

DOI:10.1039/c39910000275

upstream raw materials:

4,4'-Dibenzyloxy-3-(1,3-dioxane-2-yl)biphenyl-3'-carbaldehyde

trimethyl 2-(tert-butoxycarbonylamino)phosphonoacetate

2-benzyloxy-5-bromobenzaldehyde

2-benzyloxy-5-iodobenzaldehyde

Downstream raw materials:

benzyl 2(S)-(5-benzyloxycarbonylamino-2(S)-tert-butoxycarbonylamino-4(R)-hydroxypentanoylamino)-3-[4,4'-bisbenzyloxy-3'-(2(S)-benzyloxycarbonylamino-2-pentafluorophenyloxycarbonylethyl)biphenyl-3-yl]propionate

biphenomycin B

3-<(S)-2-(tert-Butoxycarbonylamino)-2-carboxyethyl>-4,4'-dibenzyloxy-3'-(1,3-dioxan-2-yl)biphenyl

3'-<(Z)-2-(tert-Butoxycarbonylamino)-2-carboxyvinyl>-4,4'-dibenzyloxy-3-(1,3-dioxan-2-yl)biphenyl

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