C₂₆H₃₉NO₆Si

Base Information

Chemical Name:C₂₆H₃₉NO₆Si
CAS No.:85925-72-0
Molecular Formula:C₂₆H₃₉NO₆Si
Molecular Weight:489.684
Hs Code.:

C<sub>26</sub>H<sub>39</sub>NO<sub>6</sub>Si

Synonyms:C₂₆H₃₉NO₆Si

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Chemical Property of C₂₆H₃₉NO₆Si

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Technology Process of C₂₆H₃₉NO₆Si

There total 1 articles about C₂₆H₃₉NO₆Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 5762-56-1
tris(dimethylamino)methane

: C₂₃H₃₄O₆Si

: 85925-72-0
C₂₆H₃₉NO₆Si

Guidance literature:: at 120 ℃; for 16h;
DOI:10.1021/ja00351a057

Reference yield: 99.0%

: 85925-72-0
C₂₆H₃₉NO₆Si

: 85925-73-1
C₂₄H₃₄O₇Si

Guidance literature:: With sodium acetate; In water; acetic acid; for 1h; Ambient temperature;
DOI:10.1021/ja00351a057

Reference yield:

: 85925-72-0
C₂₆H₃₉NO₆Si

: 2270-40-8,28776-47-8
4,15-diacetoxyscirpenol

Guidance literature:: Multi-step reaction with 11 steps

1: 95 percent / diisopropylethylamine / tetrahydrofuran / 96 h / Ambient temperature

2: 1.) LDA, 2.) MsCl, imidazole / 1.) THF, -78 deg C, 1 h, 2.) DMF, room temperature, 16 h

3: 90 percent / tetrahydrofuran / 1 h / -78 °C

4: 75 percent / LiAlH₄ / 1,2-dimethoxy-ethane / 1 h / Heating

5: 95 percent / pyridine / 16 h / Ambient temperature

6: 70 percent / aq. NH₄OH / methanol / 16 h / Ambient temperature

7: 90 percent / TsOH / CH₂Cl₂ / 0.17 h / Ambient temperature

8: 95 percent / pyridine / 16 h / Ambient temperature

10: 75 percent / m-chloroperbenzoic acid / CH₂Cl₂ / 2 h / 0 °C

11: 65 percent / aq. NH₄OH / methanol / 3 h / Ambient temperature

With 1H-imidazole; ammonium hydroxide; lithium aluminium tetrahydride; toluene-4-sulfonic acid; methanesulfonyl chloride; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; lithium diisopropyl amide; In tetrahydrofuran; pyridine; methanol; 1,2-dimethoxyethane; dichloromethane;
DOI:10.1021/ja00351a057