glycyl-3-cyclohexyl-D-alanylglycine

Base Information

Chemical Name:glycyl-3-cyclohexyl-D-alanylglycine
CAS No.:917577-60-7
Molecular Formula:C₁₃H₂₃N₃O₄
Molecular Weight:285.343
Hs Code.:

Synonyms:glycyl-3-cyclohexyl-D-alanylglycine

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Chemical Property of glycyl-3-cyclohexyl-D-alanylglycine

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Technology Process of glycyl-3-cyclohexyl-D-alanylglycine

There total 3 articles about glycyl-3-cyclohexyl-D-alanylglycine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₂H₃₉N₃O₆

: 917577-60-7
glycyl-3-cyclohexyl-D-alanylglycine

Guidance literature:: C₂₂H₃₉N₃O₆; With formic acid;

With ammonia; In water; at 20 ℃; pH=6 - 7;

Reference yield:

: 917577-73-2
N-(tert-butoxycarbonyl)glycyl-3-cyclohexyl-D-alanine

: 917577-60-7
glycyl-3-cyclohexyl-D-alanylglycine

Guidance literature:: Multi-step reaction with 2 steps

1.1: 4-methyl-morpholine; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate / dichloromethane / 1 h / 20 °C

2.1: formic acid

2.2: 20 °C / pH 6 - 7

With 4-methyl-morpholine; formic acid; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; In dichloromethane;

Reference yield:

: 144644-00-8
methyl (R)-2-amino-3-cyclohexylpropanoate hydrochloride

: 917577-60-7
glycyl-3-cyclohexyl-D-alanylglycine

Guidance literature:: Multi-step reaction with 4 steps

1.1: 4-methyl-morpholine; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate / dichloromethane / 0.5 h / 20 °C

1.2: 1 h / 20 °C

2.1: methanol; sodium hydroxide; water / 4 h / 20 °C

2.2: 20 °C

3.1: 4-methyl-morpholine; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate / dichloromethane / 1 h / 20 °C

4.1: formic acid

4.2: 20 °C / pH 6 - 7

With 4-methyl-morpholine; methanol; sodium hydroxide; formic acid; water; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; In dichloromethane;