1-(4-methoxy-phenyl)-4-(1,2,3,4-tetrahydroxy-butyl)-1,3-dihydro-imidazole-2-thione

Base Information

• Chemical Name: 1-(4-methoxy-phenyl)-4-(1,2,3,4-tetrahydroxy-butyl)-1,3-dihydro-imidazole-2-thione
• CAS No.: 24916-30-1
• Molecular Formula: C₁₄H₁₈N₂O₅S
• Molecular Weight: 326.373

Synonyms:1-(4-methoxy-phenyl)-4-(1,2,3,4-tetrahydroxy-butyl)-1,3-dihydro-imidazole-2-thione

Chemical Property of 1-(4-methoxy-phenyl)-4-(1,2,3,4-tetrahydroxy-butyl)-1,3-dihydro-imidazole-2-thione

Chemical Property:

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Technology Process of 1-(4-methoxy-phenyl)-4-(1,2,3,4-tetrahydroxy-butyl)-1,3-dihydro-imidazole-2-thione

There total 1 articles about 1-(4-methoxy-phenyl)-4-(1,2,3,4-tetrahydroxy-butyl)-1,3-dihydro-imidazole-2-thione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ 1-(4-methoxy-phenyl)-4-(Dr-1tf,2cf,3rf,4-tetrahydroxy-but-catf-yl)-1,3-dihydro-imidazole-2-thione (24916-30-1)

Guidance literature:

1-<4-Methoxy-anilino>-1-desoxy-D-fruktose, KSCN in sd. wss. HCl;

DOI:10.1016/0040-4020(63)85003-6

Reference yield: 80.0%

acetic anhydride (108-24-7) + 1-(4-methoxy-phenyl)-4-(1,2,3,4-tetrahydroxy-butyl)-1,3-dihydro-imidazole-2-thione (24916-30-1) → 1-(4-methoxy-phenyl)-4-(1,2,3,4-tetraacetoxy-butyl)-1,3-dihydro-imidazole-2-thione (103739-64-6)

Guidance literature:

With pyridine; at 80 ℃; for 48h;

DOI:10.1016/S0040-4020(01)81122-4

Reference yield:

acetic anhydride (108-24-7) + 1-(4-methoxy-phenyl)-4-(1,2,3,4-tetrahydroxy-butyl)-1,3-dihydro-imidazole-2-thione (24916-30-1) → Acetic acid (1R,2S,3R)-2,3,4-triacetoxy-1-[3-acetyl-1-(4-methoxy-phenyl)-2-thioxo-2,3-dihydro-1H-imidazol-4-yl]-butyl ester + 1-(4-methoxy-phenyl)-4-(1,2,3,4-tetraacetoxy-butyl)-1,3-dihydro-imidazole-2-thione (103739-64-6)

Guidance literature:

With pyridine; for 48h; Yield given. Yields of byproduct given. Title compound not separated from byproducts; Ambient temperature;

DOI:10.1016/S0040-4020(01)81122-4

Downstream raw materials:

1-(4-methoxy-phenyl)-4-(1,2,3,4-tetraacetoxy-butyl)-1,3-dihydro-imidazole-2-thione

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