bis(3-[chloro(triphenylphosphine)platino]-4-[(dimethylamino)methyl]benzyl)-[G₁]-carboxylate

Base Information

• Chemical Name: bis(3-[chloro(triphenylphosphine)platino]-4-[(dimethylamino)methyl]benzyl)-[G₁]-carboxylate
• CAS No.: 399042-63-8
• Molecular Formula: C₄₉H₄₅ClNO₄PPt
• Molecular Weight: 973.407

Synonyms:bis(3-[chloro(triphenylphosphine)platino]-4-[(dimethylamino)methyl]benzyl)-[G₁]-carboxylate

Chemical Property of bis(3-[chloro(triphenylphosphine)platino]-4-[(dimethylamino)methyl]benzyl)-[G₁]-carboxylate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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Technology Process of bis(3-[chloro(triphenylphosphine)platino]-4-[(dimethylamino)methyl]benzyl)-[G₁]-carboxylate

There total 3 articles about bis(3-[chloro(triphenylphosphine)platino]-4-[(dimethylamino)methyl]benzyl)-[G₁]-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

3-[chloro(triphenylphosphine)platino]-4-[(dimethylamino)methyl]benzyl alcohol (399042-59-2) + 3,5-dibenzyloxylbenzoyl chloride (28917-44-4) → bis(3-[chloro(triphenylphosphine)platino]-4-[(dimethylamino)methyl]benzyl)-[G1]-carboxylate (399042-63-8)

Guidance literature:

With triethyl amine; In dichloromethane; a soln. of dendron in CH2Cl2 was added to a soln. of complex and triethyl amine in CH2Cl2, the mixt. was stirred at room temp. for 3 d (N2); the mixt. was washed with aq. satd. NaCl, dried over MgSO4, filtered, evapd. in vac., the solid was washed with diethyl ether, dried in vac.; elem. anal.;

DOI:10.1021/om010500g

Reference yield:

3-[chloro(dimethylsulfoxide)platino]-4-[(dimethylamino)methyl]benzyl alcohol → bis(3-[chloro(triphenylphosphine)platino]-4-[(dimethylamino)methyl]benzyl)-[G1]-carboxylate (399042-63-8)

Guidance literature:

Multi-step reaction with 2 steps

1: dichloromethane

2: triethyl amine / dichloromethane

With triethyl amine; In dichloromethane;

DOI:10.1021/om010500g

Reference yield:

triphenylphosphine (603-35-0) → bis(3-[chloro(triphenylphosphine)platino]-4-[(dimethylamino)methyl]benzyl)-[G1]-carboxylate (399042-63-8)

Guidance literature:

Multi-step reaction with 2 steps

1: dichloromethane

2: triethyl amine / dichloromethane

With triethyl amine; In dichloromethane;

DOI:10.1021/om010500g

upstream raw materials:

3-[chloro(triphenylphosphine)platino]-4-[(dimethylamino)methyl]benzyl alcohol

3,5-dibenzyloxylbenzoyl chloride

triphenylphosphine

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