5-methyl-3-nitrosoisoxazole

Base Information

• Chemical Name: 5-methyl-3-nitrosoisoxazole
• CAS No.: 947619-95-6
• Molecular Formula: C₄H₄N₂O₂
• Molecular Weight: 112.088

Synonyms:5-methyl-3-nitrosoisoxazole

Chemical Property of 5-methyl-3-nitrosoisoxazole

Chemical Property:

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Technology Process of 5-methyl-3-nitrosoisoxazole

There total 3 articles about 5-methyl-3-nitrosoisoxazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N1-acetylsulfamethoxazole (18607-98-2) → 5-methylisoxazol-3-ylamine (1072-67-9) + 5-methyl-3-nitrosoisoxazole (947619-95-6) + N-acetylsulfanilic acid (121-62-0) + nitroso derivative of sulfamethoxazole (131549-85-4) + Benzenesulfinic acid (618-41-7) + N-(5-methyl-isoxazol-3-yl)-4-nitro-benzenesulfonamide (29699-89-6)

Guidance literature:

With sodium sulfate; In water; pH=7; pH-value; Reagent/catalyst; Kinetics; Electrochemical reaction;

DOI:10.1016/j.cclet.2020.03.073

Reference yield:

sulfamethoxazole (723-46-6) → 5-methylisoxazol-3-ylamine (1072-67-9) + 3-nitro-5-methylisoxazole (75079-82-2) + 5-methyl-3-nitrosoisoxazole (947619-95-6) + 4-amino-3-hydroxy-N- (5-methylisoxazol-3-yl)benzenesulfonamide

Guidance literature:

With iron(III) sulfate; sodium hydrogensulfite; at 25 ℃; pH=4; pH-value; Kinetics;

DOI:10.1039/d0ra05962e

Reference yield:

sulfamethoxazole (723-46-6) → 5-methylisoxazol-3-ylamine (1072-67-9) + 5-methyl-3-nitrosoisoxazole (947619-95-6) + 4-amino-3-hydroxy-N- (5-methylisoxazol-3-yl)benzenesulfonamide + 4-amino-3-hydroxy-N-(4-hydroxy-5-methylisoxazol-3-yl)benzenesulfonamide + C4H8N2O

Guidance literature:

With sodium sulfate; In water; pH=7; pH-value; Reagent/catalyst; Kinetics; Electrochemical reaction;

DOI:10.1016/j.cclet.2020.03.073

upstream raw materials:

sulfamethoxazole

N¹-acetylsulfamethoxazole

Downstream raw materials:

C₂₁H₂₃N₃O₄

C₁₁H₁₆N₂O₂

C₁₃H₁₄N₂O₂

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