4-chloro-2-nitro-5-vinyltoluene

Base Information

Chemical Name:4-chloro-2-nitro-5-vinyltoluene
CAS No.:162100-80-3
Molecular Formula:C₉H₈ClNO₂
Molecular Weight:197.621
Hs Code.:

Synonyms:4-chloro-2-nitro-5-vinyltoluene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-chloro-2-nitro-5-vinyltoluene

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Technology Process of 4-chloro-2-nitro-5-vinyltoluene

There total 2 articles about 4-chloro-2-nitro-5-vinyltoluene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 7486-35-3
tri-n-butyl(vinyl)tin

: 162100-79-0
trifluoromethanesulfonic acid 2-chloro-5-methyl-4-nitrophenyl ester

: 162100-80-3
4-chloro-2-nitro-5-vinyltoluene

Guidance literature:: With 2,6-di-tert-butyl-4-methyl-phenol; lithium chloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,4-dioxane; for 17h; Heating;
DOI:10.1021/jm970741j

Reference yield:

: 40130-97-0
2-chloro-5-methyl-4-nitro-phenol

: 162100-80-3
4-chloro-2-nitro-5-vinyltoluene

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / CH₂Cl₂ / -5 - 20 °C

2: 79 percent / LiCl, 2,6-di-tert-butyl-4-methylphenol / tetrakis(triphenylphosphine)palladium / dioxane / 17 h / Heating

With pyridine; 2,6-di-tert-butyl-4-methyl-phenol; lithium chloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,4-dioxane; dichloromethane;
DOI:10.1021/jm970741j