N-Benzyloxycarbonyl-L-prolyl-O-(2-acetamido-3,4,6-tri-O-acetyl-2-desoxy-α-D-galactopyranosyl)-L-threonyl-glycin-benzylester

Base Information

Chemical Name:N-Benzyloxycarbonyl-L-prolyl-O-(2-acetamido-3,4,6-tri-O-acetyl-2-desoxy-α-D-galactopyranosyl)-L-threonyl-glycin-benzylester
CAS No.:126133-21-9
Molecular Formula:C₄₀H₅₀N₄O₁₅
Molecular Weight:826.855
Hs Code.:

Synonyms:N-Benzyloxycarbonyl-L-prolyl-O-(2-acetamido-3,4,6-tri-O-acetyl-2-desoxy-α-D-galactopyranosyl)-L-threonyl-glycin-benzylester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-Benzyloxycarbonyl-L-prolyl-O-(2-acetamido-3,4,6-tri-O-acetyl-2-desoxy-α-D-galactopyranosyl)-L-threonyl-glycin-benzylester

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Technology Process of N-Benzyloxycarbonyl-L-prolyl-O-(2-acetamido-3,4,6-tri-O-acetyl-2-desoxy-α-D-galactopyranosyl)-L-threonyl-glycin-benzylester

There total 2 articles about N-Benzyloxycarbonyl-L-prolyl-O-(2-acetamido-3,4,6-tri-O-acetyl-2-desoxy-α-D-galactopyranosyl)-L-threonyl-glycin-benzylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1738-76-7
glycine benzyl ester p-toluenesulfonic acid salt

: 126156-02-3
N-Benzyloxycarbonyl-L-prolyl-O-(2-acetamido-3,4,6-tri-O-acetyl-2-desoxy-α-D-galactopyranosyl)-L-threonin

: 126133-21-9
N-Benzyloxycarbonyl-L-prolyl-O-(2-acetamido-3,4,6-tri-O-acetyl-2-desoxy-α-D-galactopyranosyl)-L-threonyl-glycin-benzylester

Guidance literature:: With 2-ethoxy-1-(1-ethoxycarbonyl)-1,2-dihydroquinoline; triethylamine; In dichloromethane; for 12h;

Reference yield:

: 126133-20-8
N-Benzyloxycarbonyl-L-prolyl-O-(2-acetamido-3,4,6-tri-O-acetyl-2-desoxy-α-D-galactopyranosyl)-L-threonin-tert-butylester

: 126133-21-9
N-Benzyloxycarbonyl-L-prolyl-O-(2-acetamido-3,4,6-tri-O-acetyl-2-desoxy-α-D-galactopyranosyl)-L-threonyl-glycin-benzylester

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / HCOOH / 24 h / Ambient temperature

2: 89 percent / 2-ethoxy-1-(1-ethoxycarbonyl)-1,2-dihydroquinoline, NEt₃ / CH₂Cl₂ / 12 h

With formic acid; 2-ethoxy-1-(1-ethoxycarbonyl)-1,2-dihydroquinoline; triethylamine; In dichloromethane;