C₁₆H₁₁ClO₄

Base Information

Chemical Name:C₁₆H₁₁ClO₄
CAS No.:958747-65-4
Molecular Formula:C₁₆H₁₁ClO₄
Molecular Weight:302.714
Hs Code.:

C<sub>16</sub>H<sub>11</sub>ClO<sub>4</sub>

Synonyms:C₁₆H₁₁ClO₄

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Chemical Property of C₁₆H₁₁ClO₄

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Technology Process of C₁₆H₁₁ClO₄

There total 4 articles about C₁₆H₁₁ClO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 7-hydroxy-7-methyl-3-phenyl-isochromene-6,8-dione

: 958747-65-4
C₁₆H₁₁ClO₄

Guidance literature:: With N-chloro-succinimide; In dichloromethane;
DOI:10.1021/jf300610j

Reference yield:

: 685895-45-8
2-bromo-4,6-dihydroxy-5-methylbenzaldehyde

: 958747-65-4
C₁₆H₁₁ClO₄

Guidance literature:: Multi-step reaction with 3 steps

1.1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / N,N-dimethyl-formamide / 0.17 h / Inert atmosphere

1.2: 60 °C / Inert atmosphere

2.1: silver nitrate; trifluoroacetic acid / 1,2-dichloro-ethane / 0.08 h / 20 °C

2.2: 1 h / 20 °C

3.1: N-chloro-succinimide / dichloromethane

With bis-triphenylphosphine-palladium(II) chloride; N-chloro-succinimide; copper(l) iodide; silver nitrate; triethylamine; trifluoroacetic acid; In dichloromethane; 1,2-dichloro-ethane; N,N-dimethyl-formamide; 1.1: Sonogashira coupling / 1.2: Sonogashira coupling;
DOI:10.1021/jf300610j

Reference yield:

: 685895-61-8
2,4-dihydroxy-3-methyl-6-phenylethynyl-benzaldehyde

: 958747-65-4
C₁₆H₁₁ClO₄

Guidance literature:: Multi-step reaction with 2 steps

1.1: silver nitrate; trifluoroacetic acid / 1,2-dichloro-ethane / 0.08 h / 20 °C

1.2: 1 h / 20 °C

2.1: N-chloro-succinimide / dichloromethane

With N-chloro-succinimide; silver nitrate; trifluoroacetic acid; In dichloromethane; 1,2-dichloro-ethane;
DOI:10.1021/jf300610j