allyl (3-(2-nitrophenylsulfonamido)propyl)(3-(2,2,2-trifluoroacetamido)propyl)carbamate

Base Information

Chemical Name:allyl (3-(2-nitrophenylsulfonamido)propyl)(3-(2,2,2-trifluoroacetamido)propyl)carbamate
CAS No.:380235-20-1
Molecular Formula:C₁₈H₂₃F₃N₄O₇S
Molecular Weight:496.464
Hs Code.:

Synonyms:allyl (3-(2-nitrophenylsulfonamido)propyl)(3-(2,2,2-trifluoroacetamido)propyl)carbamate

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Chemical Property of allyl (3-(2-nitrophenylsulfonamido)propyl)(3-(2,2,2-trifluoroacetamido)propyl)carbamate

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Technology Process of allyl (3-(2-nitrophenylsulfonamido)propyl)(3-(2,2,2-trifluoroacetamido)propyl)carbamate

There total 6 articles about allyl (3-(2-nitrophenylsulfonamido)propyl)(3-(2,2,2-trifluoroacetamido)propyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 2937-50-0
Allyl chloroformate

: 2,2,2-trifluoro-N-{3-[3-(2-nitro-benzenesulfonylamino)-propylamino]-propyl}-acetamide; compound with trifluoro-acetic acid

: 380235-20-1
allyl (3-(2-nitrophenylsulfonamido)propyl)(3-(2,2,2-trifluoroacetamido)propyl)carbamate

Guidance literature:: With sodium hydrogencarbonate; In 1,4-dioxane; water; at 20 ℃;
DOI:10.1021/ol0101741

Reference yield:

: C₁₄H₁₉F₃N₄O₅S*3C₂HF₃O₂

: 2937-50-0
Allyl chloroformate

: 380235-20-1
allyl (3-(2-nitrophenylsulfonamido)propyl)(3-(2,2,2-trifluoroacetamido)propyl)carbamate

Guidance literature:: With sodium hydrogencarbonate; In 1,4-dioxane; water; Cooling with ice;
DOI:10.1016/j.tet.2014.04.084

Reference yield:

: 444108-27-4
N-[3-(3-amino-propylamino)-propyl]-2-nitro-benzenesulfonamide

: 380235-20-1
allyl (3-(2-nitrophenylsulfonamido)propyl)(3-(2,2,2-trifluoroacetamido)propyl)carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: H₂O / acetonitrile / 16 h / Heating

2: 85 percent / NaHCO₃ / H₂O; dioxane / 4 h / 20 °C

With water; sodium hydrogencarbonate; In 1,4-dioxane; water; acetonitrile;
DOI:10.1021/ol0101741