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C25H26BrNO3

Base Information
  • Chemical Name:C25H26BrNO3
  • CAS No.:935764-62-8
  • Molecular Formula:C25H26BrNO3
  • Molecular Weight:468.39
  • Hs Code.:
C<sub>25</sub>H<sub>26</sub>BrNO<sub>3</sub>

Synonyms:C25H26BrNO3

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Chemical Property of C25H26BrNO3
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Technology Process of C25H26BrNO3

There total 1 articles about C25H26BrNO3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In toluene; at 80 ℃; for 1.5h; Resolution of racemate;
Guidance literature:
With hydrogen bromide; In ethyl acetate; at 25 ℃; for 0.75h;
Guidance literature:
Multi-step reaction with 6 steps
1.1: hydrogen bromide / ethyl acetate / 0.75 h / 25 °C
2.1: (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0.33 h / 25 °C
3.1: hydrogen / palladium 10% on activated carbon / methanol; dichloromethane / 7 h / 25 °C
4.1: pyridine / dichloromethane; allyl alcohol / 16 h / 20 °C
5.1: hydrogen bromide / ethyl acetate / 0.75 h / 25 °C
5.2: 0.42 h / 25 °C
6.1: hydrogen / palladium 10% on activated carbon / methanol
With pyridine; hydrogen bromide; hydrogen; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; palladium 10% on activated carbon; In methanol; dichloromethane; ethyl acetate; allyl alcohol; N,N-dimethyl-formamide;
upstream raw materials:

C25H25BrINO3

Downstream raw materials:

BrH*C20H18BrNO

C34H32BrN3O4

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