Technology Process of C25H26BrNO3
There total 1 articles about C25H26BrNO3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride;
In
toluene;
at 80 ℃;
for 1.5h;
Resolution of racemate;
- Guidance literature:
-
With
hydrogen bromide;
In
ethyl acetate;
at 25 ℃;
for 0.75h;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: hydrogen bromide / ethyl acetate / 0.75 h / 25 °C
2.1: (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0.33 h / 25 °C
3.1: hydrogen / palladium 10% on activated carbon / methanol; dichloromethane / 7 h / 25 °C
4.1: pyridine / dichloromethane; allyl alcohol / 16 h / 20 °C
5.1: hydrogen bromide / ethyl acetate / 0.75 h / 25 °C
5.2: 0.42 h / 25 °C
6.1: hydrogen / palladium 10% on activated carbon / methanol
With
pyridine; hydrogen bromide; hydrogen; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine;
palladium 10% on activated carbon;
In
methanol; dichloromethane; ethyl acetate; allyl alcohol; N,N-dimethyl-formamide;