2-(benzyl(phenylethynyl)amino)-5,5-dimethyl-1,3,2-dioxaphosphinane 2-oxide

Base Information

Chemical Name:2-(benzyl(phenylethynyl)amino)-5,5-dimethyl-1,3,2-dioxaphosphinane 2-oxide
CAS No.:1645293-03-3
Molecular Formula:C₂₀H₂₂NO₃P
Molecular Weight:355.373
Hs Code.:

Synonyms:2-(benzyl(phenylethynyl)amino)-5,5-dimethyl-1,3,2-dioxaphosphinane 2-oxide

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Chemical Property of 2-(benzyl(phenylethynyl)amino)-5,5-dimethyl-1,3,2-dioxaphosphinane 2-oxide

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Technology Process of 2-(benzyl(phenylethynyl)amino)-5,5-dimethyl-1,3,2-dioxaphosphinane 2-oxide

There total 1 articles about 2-(benzyl(phenylethynyl)amino)-5,5-dimethyl-1,3,2-dioxaphosphinane 2-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 827348-43-6
2-(benzylamino)-5,5-dimethyl-1,3,2-dioxaphosphinane 2-oxide

: 932-87-6
1-Bromo-2-phenylacetylene

: 1645293-03-3
2-(benzyl(phenylethynyl)amino)-5,5-dimethyl-1,3,2-dioxaphosphinane 2-oxide

Guidance literature:: With potassium phosphate; 1,10-Phenanthroline; copper(ll) sulfate pentahydrate; In toluene; at 95 ℃; for 21h; Inert atmosphere;
DOI:10.1002/chem.201402653

Reference yield: 93.0%

: 1645293-03-3
2-(benzyl(phenylethynyl)amino)-5,5-dimethyl-1,3,2-dioxaphosphinane 2-oxide

: 670-54-2
ethenetetracarbonitrile

: 1645293-06-6
C₂₆H₂₂N₅O₃P

Guidance literature:: In dichloromethane; at 20 ℃; for 6.5h;
DOI:10.1002/chem.201402653

Reference yield: 92.0%

: 1645293-03-3
2-(benzyl(phenylethynyl)amino)-5,5-dimethyl-1,3,2-dioxaphosphinane 2-oxide

: C₁₁H₈N₄S

: C₂₆H₂₅N₄O₃PS

Guidance literature:: With dichloro(2-picolinato)gold(III); In 1,2-dichloro-benzene; at 125 ℃; for 1h; Inert atmosphere; Schlenk technique;
DOI:10.1002/adsc.201700249