Technology Process of C14H11BrFNO2
There total 6 articles about C14H11BrFNO2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
dipyridinium dichromate;
In
dichloromethane;
at 20 ℃;
for 4h;
Inert atmosphere;
DOI:10.1021/ml2000438
- Guidance literature:
-
Multi-step reaction with 4 steps
1: water; sodium hydroxide / methanol / 16 h / 20 °C / Inert atmosphere
2: pyridine; trifluoro-[1,3,5]triazine / dichloromethane / -10 - 20 °C / Inert atmosphere
3: sodium tetrahydroborate / methanol; dichloromethane / 2 h / 20 °C / Inert atmosphere
4: dipyridinium dichromate / dichloromethane / 4 h / 20 °C / Inert atmosphere
With
pyridine; sodium tetrahydroborate; dipyridinium dichromate; trifluoro-[1,3,5]triazine; water; sodium hydroxide;
In
methanol; dichloromethane;
DOI:10.1021/ml2000438
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium tetrahydroborate / methanol; dichloromethane / 2 h / 20 °C / Inert atmosphere
2: dipyridinium dichromate / dichloromethane / 4 h / 20 °C / Inert atmosphere
With
sodium tetrahydroborate; dipyridinium dichromate;
In
methanol; dichloromethane;
DOI:10.1021/ml2000438